{((CH₃)2CHNCHCHNCH(CH₃)2)Fe(CNC₆H₁₁)3}

Base Information

Chemical Name:{((CH₃)2CHNCHCHNCH(CH₃)2)Fe(CNC₆H₁₁)3}
CAS No.:147244-64-2
Molecular Formula:C₂₉H₄₉FeN₅
Molecular Weight:523.589
Hs Code.:

{((CH<sub>3</sub>)2CHNCHCHNCH(CH<sub>3</sub>)2)Fe(CNC<sub>6</sub>H<sub>11</sub>)3}

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Chemical Property of {((CH₃)2CHNCHCHNCH(CH₃)2)Fe(CNC₆H₁₁)3}

Chemical Property:

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Technology Process of {((CH₃)2CHNCHCHNCH(CH₃)2)Fe(CNC₆H₁₁)3}

There total 1 articles about {((CH₃)2CHNCHCHNCH(CH₃)2)Fe(CNC₆H₁₁)3} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 931-53-3
Cyclohexyl isocyanide

: 62801-15-4
Fe((CH₃)2CHNCHCHNCH(CH₃)2)2

: 147244-64-2
{((CH₃)2CHNCHCHNCH(CH₃)2)Fe(CNC₆H₁₁)3}

Guidance literature:: In pentane; addn. of isocyanide to stirred Fe complex soln. under N2; reacting, 30 min; filtration; not isolated; purification by subliming free isocyanide and diimine by gentle heating; detn. by 1H and 13C NMR, MS and IR;

Reference yield:

: 147244-64-2
{((CH₃)2CHNCHCHNCH(CH₃)2)Fe(CNC₆H₁₁)3}

: 762-42-5
dimethyl acetylenedicarboxylate

: 147244-66-4
Fe(CNC₆H₁₁)3(C₆H₂N₂(CH(CH₃)2)2(CO₂CH₃)4)

Guidance literature:: In pentane; addn. of dimethyl acetylenedicarboxylate soln. (diethyl ether/pentane) to Fe complex soln. (pentane) under N2, -78°C, 45 min; pptn.; washing (cold pentane); drying (vac.); chromy. (silica, diethyl ether); elem. anal.;

Reference yield:

: 147244-64-2
{((CH₃)2CHNCHCHNCH(CH₃)2)Fe(CNC₆H₁₁)3}

: 624-48-6
dimethyl cis-but-2-ene-1,4-dioate

: 96019-01-1
tetramethyl (Z)-2-butene-1,2,3,4-tetracarboxylate

: Fe(CNC₆H₁₁)3(C₆H₃N₂(CH(CH₃)2)2(CO₂CH₃)2(CH₂CO₂CH₃)(O))

Guidance literature:: In diethyl ether; pentane; addn. of dimethyl maleate soln. (diethyl ether/pentane) to Fe complex soln. (pentane) under N2, 243 K, 1h; stirring, 2h; pptn.; washing (pentane); drying (vac.); dissoln. (diethyl ether/CH2Cl2); chromy. (silica gel, pentane, diethyl ether, diethyl ether/CH2Cl2 5/1); evapn.; product ratio butenecarboxylate/Fe complex = 20/80; total yield 50%; elem. anal.;
DOI:10.1021/om00026a031