3-(4'-Acetoxyphenyl)-naphthalin-1,2,4-triyl-triacetat

Base Information

• Chemical Name: 3-(4'-Acetoxyphenyl)-naphthalin-1,2,4-triyl-triacetat
• CAS No.: 54808-10-5
• Molecular Formula: C₂₄H₂₀O₈
• Molecular Weight: 436.418
• Mol file: 54808-10-5.mol

Synonyms:

Chemical Property of 3-(4'-Acetoxyphenyl)-naphthalin-1,2,4-triyl-triacetat

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3-(4'-Acetoxyphenyl)-naphthalin-1,2,4-triyl-triacetat

There total 4 articles about 3-(4'-Acetoxyphenyl)-naphthalin-1,2,4-triyl-triacetat which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

p-methylanizole (104-93-8) → 3-(4'-Acetoxyphenyl)-naphthalin-1,2,4-triyl-triacetat (54808-10-5)

Guidance literature:

Multi-step reaction with 4 steps

1: (tBuO)2 / Heating

2: (oxidation)

3: Zn, NaOAc

4: (i) Py*HCl, (heating), (ii) /BRN= 385737/, Zn, NaOAc

With di-tert-butyl peroxide; sodium acetate; zinc;

Reference yield:

2-hydroxy-3-(4-methoxybenzyl)naphthalene-1,4-dione (59304-99-3) → 3-(4'-Acetoxyphenyl)-naphthalin-1,2,4-triyl-triacetat (54808-10-5)

Guidance literature:

Multi-step reaction with 3 steps

1: (oxidation)

2: Zn, NaOAc

3: (i) Py*HCl, (heating), (ii) /BRN= 385737/, Zn, NaOAc

With sodium acetate; zinc;

Reference yield:

1,4-dihydro-2-hydroxy-3-(4-methoxyphenyl)-1,4-naphthalenedione (54808-21-8) → 3-(4'-Acetoxyphenyl)-naphthalin-1,2,4-triyl-triacetat (54808-10-5)

Guidance literature:

Multi-step reaction with 2 steps

1: Zn, NaOAc

2: (i) Py*HCl, (heating), (ii) /BRN= 385737/, Zn, NaOAc

With sodium acetate; zinc;

upstream raw materials:

Acetic acid 1,4-diacetoxy-3-(4-methoxy-phenyl)-naphthalen-2-yl ester

acetic anhydride

p-methylanizole

2-hydroxy-3-(4-methoxybenzyl)naphthalene-1,4-dione