(2,3,7,8,12,13,17,18-octamethyl-5,10,15,20-tetraphenylporphyrin)iron(III) perchlorate

Base Information

Chemical Name:(2,3,7,8,12,13,17,18-octamethyl-5,10,15,20-tetraphenylporphyrin)iron(III) perchlorate
CAS No.:733752-08-4
Molecular Formula:C₅₂H₄₄FeN₄*ClO₄
Molecular Weight:880.246
Hs Code.:

Synonyms:

Suppliers and Price of (2,3,7,8,12,13,17,18-octamethyl-5,10,15,20-tetraphenylporphyrin)iron(III) perchlorate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (2,3,7,8,12,13,17,18-octamethyl-5,10,15,20-tetraphenylporphyrin)iron(III) perchlorate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (2,3,7,8,12,13,17,18-octamethyl-5,10,15,20-tetraphenylporphyrin)iron(III) perchlorate

There total 1 articles about (2,3,7,8,12,13,17,18-octamethyl-5,10,15,20-tetraphenylporphyrin)iron(III) perchlorate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 186910-32-7
[Fe(2,3,7,8,12,13,17,18-octamethyl-5,10,15,20-tetraphenylporphyrin)Cl]

: silver perchlorate

: 733752-08-4
(2,3,7,8,12,13,17,18-octamethyl-5,10,15,20-tetraphenylporphyrin)iron(III) perchlorate

Guidance literature:: In tetrahydrofuran; Fe complex dissolved in THF, heated, AgClO4 in THF added, refluxed for 15 min; cooled to room temp., filtered, toluene added, evapd. (vac., 50°C), dissolved in boiling toluene, boiling heptane added, crystd. for 1 d,filtered, washed (cold heptane), dried (vac., 60°C, 4 h); obtain ed as contg. toluene;
DOI:10.1021/ic035010q

Reference yield:

: 100-48-1
pyridine-4-carbonitrile

: 733752-08-4
(2,3,7,8,12,13,17,18-octamethyl-5,10,15,20-tetraphenylporphyrin)iron(III) perchlorate

: 658045-62-6
iron(III) octamethyltetraphenylporphyrin bis(4-cyanopyridine) perchlorate

Guidance literature:: In dichloromethane-d2; a soln. of Fe complex added to ligand, heated, more ligand added; not isolated, detected by NMR;
DOI:10.1021/ic035010q

Reference yield:

: 733752-08-4
(2,3,7,8,12,13,17,18-octamethyl-5,10,15,20-tetraphenylporphyrin)iron(III) perchlorate

: 119072-55-8,7188-38-7
tert-butylisonitrile

: 353749-98-1
bis(tert-butylisocyanide)[(2,3,7,8,12,13,17,18-octamethyl-5,10,15,20-tetraphenylporphyrinato)iron(III)] perchlorate

Guidance literature:: In dichloromethane-d2; 3-6 equiv of isocyanide was added to a soln. of complex in CD2Cl2; concd., layered with o-xylene or dodecane in the capped tubes protected from light for 7-10 days;