[Cu₂(PhP(C₆H₄S-2)2)(PPh₃)2(acetonitrile)]

Base Information

Chemical Name:[Cu₂(PhP(C₆H₄S-2)2)(PPh₃)2(acetonitrile)]
CAS No.:1234906-89-8
Molecular Formula:C₅₆H₄₆Cu₂NP₃S₂
Molecular Weight:1017.13
Hs Code.:

[Cu<sub>2</sub>(PhP(C<sub>6</sub>H<sub>4</sub>S-2)2)(PPh<sub>3</sub>)2(acetonitrile)]

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Chemical Property of [Cu₂(PhP(C₆H₄S-2)2)(PPh₃)2(acetonitrile)]

Chemical Property:

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Technology Process of [Cu₂(PhP(C₆H₄S-2)2)(PPh₃)2(acetonitrile)]

There total 1 articles about [Cu₂(PhP(C₆H₄S-2)2)(PPh₃)2(acetonitrile)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 12775-96-1,15158-11-9,15721-63-8,16941-75-6,17493-86-6,19498-52-3,20499-83-6,20499-84-7,20499-85-8,20499-86-9,20573-10-8,20573-11-9,21595-51-7,21595-52-8,22206-52-6,26445-28-3,28959-95-7,37362-93-9,39417-05-5,54603-16-6,54603-23-5,54603-32-6,54603-40-6,54603-48-4,54603-81-5,54603-89-3,56316-56-4,95985-91-4,122297-32-9,7440-50-8
copper

: 119327-18-3
bis(phenyl-2-thiol)phenylphosphine

: 603-35-0
triphenylphosphine

: 75-05-8,26809-02-9
acetonitrile

: 1234906-89-8
[Cu₂(PhP(C₆H₄S-2)2)(PPh₃)2(acetonitrile)]

: [Cu₂(PhP(C₆H₄S-2)2)(PPh₃)2(acetonitrile)]*3acetonitrile

Guidance literature:: With (CH₃)4NClO₄; In acetonitrile; Electrolysis; under N2; soln. of PhP(C6H4SH-2)2 (0.190 mmol) and PPh3 (0.380 mmol) electrolyzed in the presence of Me4NClO4 using Cu anode (12 V, 10 mA, 1 h);Cu (24.4 mg) dissolved from anode (E(f) = 1.0 mol/F); solid isolated, washed with diethyl ether, dried under vac.; elem. anal.; crystals of solvate obtained by slow concn. of mother liquor;
DOI:10.1002/ejic.200900941