1L-N¹-benzyloxycarbonyl-O⁶-[2-benzyloxycarbonylamino-O⁴,O⁶-bis-(naphthalene-1-carbonyl)-α-D-ribo-2,3-dideoxy-hexopyranosyl]-N³,O⁴-carbonyl-O⁵-methanesulfonyl-2-deoxy-streptamine

Base Information

• Chemical Name: 1L-N¹-benzyloxycarbonyl-O⁶-[2-benzyloxycarbonylamino-O⁴,O⁶-bis-(naphthalene-1-carbonyl)-α-D-ribo-2,3-dideoxy-hexopyranosyl]-N³,O⁴-carbonyl-O⁵-methanesulfonyl-2-deoxy-streptamine
• CAS No.: 65456-90-8
• Molecular Formula: C₅₂H₄₉N₃O₁₅S
• Molecular Weight: 988.038

Synonyms:

Chemical Property of 1L-N¹-benzyloxycarbonyl-O⁶-[2-benzyloxycarbonylamino-O⁴,O⁶-bis-(naphthalene-1-carbonyl)-α-D-ribo-2,3-dideoxy-hexopyranosyl]-N³,O⁴-carbonyl-O⁵-methanesulfonyl-2-deoxy-streptamine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1L-N¹-benzyloxycarbonyl-O⁶-[2-benzyloxycarbonylamino-O⁴,O⁶-bis-(naphthalene-1-carbonyl)-α-D-ribo-2,3-dideoxy-hexopyranosyl]-N³,O⁴-carbonyl-O⁵-methanesulfonyl-2-deoxy-streptamine

There total 3 articles about 1L-N¹-benzyloxycarbonyl-O⁶-[2-benzyloxycarbonylamino-O⁴,O⁶-bis-(naphthalene-1-carbonyl)-α-D-ribo-2,3-dideoxy-hexopyranosyl]-N³,O⁴-carbonyl-O⁵-methanesulfonyl-2-deoxy-streptamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1D-N,N'-bis-benzyloxycarbonyl-O4-(2-benzyloxycarbonylamino-α-D-ribo-2,3-dideoxy-hexopyranosyl)-2-deoxy-streptamine (63532-10-5,73522-55-1) → 1L-N1-benzyloxycarbonyl-O6-[2-benzyloxycarbonylamino-O4,O6-bis-(naphthalene-1-carbonyl)-α-D-ribo-2,3-dideoxy-hexopyranosyl]-N3,O4-carbonyl-O5-methanesulfonyl-2-deoxy-streptamine (65456-90-8)

Guidance literature:

Multi-step reaction with 2 steps

1: (i) NaH, DMF, (ii) /BRN= 775785/, Py

2: Py / Ambient temperature

With pyridine;

DOI:10.1246/bcsj.50.2369

Reference yield:

naphthalene-1-carbonic acid chloride (879-18-5) → 1L-N1-benzyloxycarbonyl-O6-[2-benzyloxycarbonylamino-O4,O6-bis-(naphthalene-1-carbonyl)-α-D-ribo-2,3-dideoxy-hexopyranosyl]-N3,O4-carbonyl-O5-methanesulfonyl-2-deoxy-streptamine (65456-90-8)

Guidance literature:

Multi-step reaction with 2 steps

1: (i) NaH, DMF, (ii) /BRN= 775785/, Py

2: Py / Ambient temperature

With pyridine;

DOI:10.1246/bcsj.50.2369

Reference yield:

1L-N1-benzyloxycarbonyl-O6-[2-benzyloxycarbonylamino-O4,O6-bis-(naphthalene-1-carbonyl)-α-D-ribo-2,3-dideoxy-hexopyranosyl]-N3,O4-carbonyl-2-deoxy-streptamine (65456-89-5) + methanesulfonyl chloride (124-63-0) → 1L-N1-benzyloxycarbonyl-O6-[2-benzyloxycarbonylamino-O4,O6-bis-(naphthalene-1-carbonyl)-α-D-ribo-2,3-dideoxy-hexopyranosyl]-N3,O4-carbonyl-O5-methanesulfonyl-2-deoxy-streptamine (65456-90-8)

Guidance literature:

With pyridine; Ambient temperature;

DOI:10.1246/bcsj.50.2369

upstream raw materials:

1L-N¹-benzyloxycarbonyl-O⁶-[2-benzyloxycarbonylamino-O⁴,O⁶-bis-(naphthalene-1-carbonyl)-α-D-ribo-2,3-dideoxy-hexopyranosyl]-N³,O⁴-carbonyl-2-deoxy-streptamine

methanesulfonyl chloride

1D-N,N'-bis-benzyloxycarbonyl-O⁴-(2-benzyloxycarbonylamino-α-D-ribo-2,3-dideoxy-hexopyranosyl)-2-deoxy-streptamine

naphthalene-1-carbonic acid chloride

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