3-[4-(3-Hydrazinyl-3-oxoprop-1-enyl)phenyl]prop-2-enehydrazide

Base Information

• Chemical Name: 3-[4-(3-Hydrazinyl-3-oxoprop-1-enyl)phenyl]prop-2-enehydrazide
• CAS No.: 52172-63-1
• Molecular Formula: C₁₂H₁₄N₄O₂
• Molecular Weight: 246.269
• DSSTox Substance ID: DTXSID601204748
• Mol file: 52172-63-1.mol

Synonyms:52172-63-1;DTXSID601204748;AKOS004900724;2-Propenoic acid, 3,3'-(1,4-phenylene)bis-, dihydrazide

Chemical Property of 3-[4-(3-Hydrazinyl-3-oxoprop-1-enyl)phenyl]prop-2-enehydrazide

Chemical Property:

• XLogP3: -0.2
• Hydrogen Bond Donor Count: 4
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 4
• Exact Mass: 246.11167570
• Heavy Atom Count: 18
• Complexity: 310

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: C1=CC(=CC=C1C=CC(=O)NN)C=CC(=O)NN

Technology Process of 3-[4-(3-Hydrazinyl-3-oxoprop-1-enyl)phenyl]prop-2-enehydrazide

There total 3 articles about 3-[4-(3-Hydrazinyl-3-oxoprop-1-enyl)phenyl]prop-2-enehydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

diethyl (2E,2′E)-3,3′-benzene-1,4-diylbis-prop-2-enoate (23746-57-8) → 3t,3't-p-phenylene-di-acrylic acid dihydrazide (52172-63-1)

Guidance literature:

With ethanol; hydrazine hydrate;

DOI:10.1002/hlca.194102401108

Reference yield:

1,4-phenylenediacrylic acid (23713-85-1) → 3t,3't-p-phenylene-di-acrylic acid dihydrazide (52172-63-1)

Guidance literature:

Multi-step reaction with 2 steps

1: phosphorus (V)-chloride / anschliessendes Behandeln mit Aethanol

2: ethanol; hydrazine hydrate

With ethanol; phosphorus pentachloride; hydrazine hydrate;

DOI:10.1002/hlca.194102401108

Reference yield:

terephthalaldehyde, (623-27-8) → 3t,3't-p-phenylene-di-acrylic acid dihydrazide (52172-63-1)

Guidance literature:

Multi-step reaction with 3 steps

1: pyridine; piperidine

2: phosphorus (V)-chloride / anschliessendes Behandeln mit Aethanol

3: ethanol; hydrazine hydrate

With piperidine; pyridine; ethanol; phosphorus pentachloride; hydrazine hydrate;

DOI:10.1002/hlca.194102401108

upstream raw materials:

diethyl (2E,2′E)-3,3′-benzene-1,4-diylbis-prop-2-enoate

1,4-phenylenediacrylic acid

terephthalaldehyde,