1-(4-Nitrophenyl)-5-styryltetrazole

Base Information

• Chemical Name: 1-(4-Nitrophenyl)-5-styryltetrazole
• CAS No.: 74941-74-5
• Molecular Formula: C₁₅H₁₁N₅O₂
• Molecular Weight: 293.285
• Mol file: 74941-74-5.mol

Synonyms:

Chemical Property of 1-(4-Nitrophenyl)-5-styryltetrazole

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-(4-Nitrophenyl)-5-styryltetrazole

There total 2 articles about 1-(4-Nitrophenyl)-5-styryltetrazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

1-phenyl-5-(β-styryl)tetrazole (66655-46-7) → 1-(4-Nitrophenyl)-5-styryltetrazole (74941-74-5) + 1-(4-Nitrophenyl)-5-(4-nitrostyryl)tetrazole (74941-75-6)

Guidance literature:

With sulfuric acid; nitric acid; at 15 ℃; Product distribution; other temp. (45-50 deg C);

DOI:10.1007/BF00552790

Reference yield:

β-Phenylacrylic acid 4-nitroanilide (134430-90-3,74948-33-7) → 1-(4-Nitrophenyl)-5-styryltetrazole (74941-74-5)

Guidance literature:

With tris-(2-chloro-ethyl)-amine; phosphorus pentachloride; Yield given. Multistep reaction; 1) C₆H₆, 60 - 80 deg C; 2) 12 h, 20 deg C; 3) 6 h reflux;

DOI:10.1007/BF00552790

upstream raw materials:

1-phenyl-5-(β-styryl)tetrazole

β-Phenylacrylic acid 4-nitroanilide