VOCl₃(C₅NH₄NHCSNHC₆H₅)

Base Information

• Chemical Name: VOCl₃(C₅NH₄NHCSNHC₆H₅)
• CAS No.: 80291-21-0
• Molecular Formula: C₁₂H₁₁Cl₃N₃OSV
• Molecular Weight: 402.605
• Mol file: 80291-21-0.mol

Synonyms:

Chemical Property of VOCl₃(C₅NH₄NHCSNHC₆H₅)

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of VOCl₃(C₅NH₄NHCSNHC₆H₅)

There total 1 articles about VOCl₃(C₅NH₄NHCSNHC₆H₅) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-(2'-pyridyl)-3-phenylthiourea (886-60-2) + vanadium(V) oxychloride (7727-18-6) → VOCl3(C5NH4NHCSNHC6H5) (80291-21-0)

Guidance literature:

In tetrachloromethane; chloroform; to ligand in CHCl3/CCl4 mixt. added drop by drop CCl4 soln. VOCl3 with stirring and ice-cooling, mixt. shaken and allowed to stand for 8 h; complex filtered, washed with CCl4 and CHCl3; elem. anal.;

DOI:10.1016/S0277-5387(00)81088-8

upstream raw materials:

1-(2'-pyridyl)-3-phenylthiourea

vanadium(V) oxychloride