1-hydroxy-3-cyclohexylaminopropylidenediphosphonic acid

Base Information

Chemical Name:1-hydroxy-3-cyclohexylaminopropylidenediphosphonic acid
CAS No.:114084-71-8
Molecular Formula:C₉H₂₁NO₇P₂
Molecular Weight:317.216
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-hydroxy-3-cyclohexylaminopropylidenediphosphonic acid

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Technology Process of 1-hydroxy-3-cyclohexylaminopropylidenediphosphonic acid

There total 2 articles about 1-hydroxy-3-cyclohexylaminopropylidenediphosphonic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 26872-84-4
N-cyclohexyl-3-aminopropionic acid

: 114084-71-8
1-hydroxy-3-cyclohexylaminopropylidenediphosphonic acid

Guidance literature:: With phosphoric acid; water; phosphorus trichloride; Yield given; Multistep reaction; 1.) chlorobenzene, 100-105 deg C, 3 h, 2.) reflux, 1 h;
DOI:10.1007/BF02495695

Reference yield:

: 108-91-8,157973-60-9
cyclohexylamine

: 114084-71-8
1-hydroxy-3-cyclohexylaminopropylidenediphosphonic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 68 percent / 48 h / 20 °C

2: 1.) H₃PO₄, PCl₃, 2.) H₂O / 1.) chlorobenzene, 100-105 deg C, 3 h, 2.) reflux, 1 h

With phosphoric acid; water; phosphorus trichloride;
DOI:10.1007/BF02495695