2,6-bis(N-methyl-N-phenyl-N-chloromethylammonium)octahydro-closo-decaborane

Base Information

Chemical Name:2,6-bis(N-methyl-N-phenyl-N-chloromethylammonium)octahydro-closo-decaborane
CAS No.:947136-71-2
Molecular Formula:C₁₆H₂₈B₁₀Cl₂N₂
Molecular Weight:427.428
Hs Code.:

Synonyms:

Suppliers and Price of 2,6-bis(N-methyl-N-phenyl-N-chloromethylammonium)octahydro-closo-decaborane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,6-bis(N-methyl-N-phenyl-N-chloromethylammonium)octahydro-closo-decaborane

Chemical Property:

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Technology Process of 2,6-bis(N-methyl-N-phenyl-N-chloromethylammonium)octahydro-closo-decaborane

There total 1 articles about 2,6-bis(N-methyl-N-phenyl-N-chloromethylammonium)octahydro-closo-decaborane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: bis(tetrabutylammonium)-decahydro-closo-decaborate

: 93-61-8
N-methyl-N-phenylformamide

: 10025-87-3,12599-09-6,63736-95-8,39380-77-3
trichlorophosphate

: 947136-71-2
2,6-bis(N-methyl-N-phenyl-N-chloromethylammonium)octahydro-closo-decaborane

: 947136-70-1
2,7-bis(N-methyl-N-phenyl-N-chloromethylammonium)octahydro-closo-decaborane

Guidance literature:: In acetonitrile; soln. of (Bu4N)2B10H10, MeCN and substituted formamide kept for 1 h in ice bath under vigorous stirring; POCl3 added dropwise in such way as to prevent the heating of mixt. above 5°C; after 30-60 min warmed toroom temp.; heated at 60°C...; after 1-2 h cooled in air to room temp.; H2O with ice added; pH adjustedto 6 (aq. NaOH); extd. (CH2Cl2); extracts evapd. in rotary evaporator a t 25°C (100 mbar) and then in vac.; mixt. applied to column packed with silica gel (CHCl3 as eluent)..;
DOI:10.1134/S003602360610007X