Di-tert-butylphosphinous iodide

Base Information

• Chemical Name: Di-tert-butylphosphinous iodide
• CAS No.: 66783-70-8
• Molecular Formula: C₈H₁₈IP
• Molecular Weight: 272.109

Synonyms:

Chemical Property of Di-tert-butylphosphinous iodide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Di-tert-butylphosphinous iodide

There total 1 articles about Di-tert-butylphosphinous iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

[Li+*3DME][Cl((2,6-iPr2C6H3)N)2W(η2-t-Bu2PP)-] + iodine (7553-56-2,12190-71-5,8031-47-8) → (1,2-η2-tBu2PPPtBu2)W(2,6-iPr2C6H3N)2Cl (1610790-71-0) + C32H53ClN2P2W + (1,2-η2-tBu2PPPtBu2)W(2,6-iPr2C6H3N)2I + Di-tert-butylphosphinous iodide (66783-70-8)

Guidance literature:

In 1,2-dimethoxyethane; at -40 - 20 ℃; for 24h; Schlenk technique;

DOI:10.1021/acs.inorgchem.5b01063

Reference yield:

Di-tert-butylphosphinous iodide (66783-70-8) + iodomethylbenzene (620-05-3) → C15H25IP(1+)*I(1-)

Guidance literature:

In [D₃]acetonitrile; at 20 ℃; for 15h; Inert atmosphere;

DOI:10.1021/acs.organomet.5b00671

upstream raw materials:

iodine

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