Thr(CH2Ph)-Dopa(diCH2Ph)-Lys2(Cl)> p-nitrophenyl ester hydrochloride

Base Information

Chemical Name:Thr(CH2Ph)-Dopa(diCH2Ph)-Lys2(Cl)> p-nitrophenyl ester hydrochloride
CAS No.:111122-60-2
Molecular Formula:C₅₄H₅₆ClN₅O₁₁*ClH
Molecular Weight:1022.98
Hs Code.:

Thr(CH2Ph)-Dopa(diCH2Ph)-Lys<Z<sup>2</sup>(Cl)> p-nitrophenyl ester hydrochloride

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Chemical Property of Thr(CH2Ph)-Dopa(diCH2Ph)-Lys2(Cl)> p-nitrophenyl ester hydrochloride

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Technology Process of Thr(CH2Ph)-Dopa(diCH2Ph)-Lys2(Cl)> p-nitrophenyl ester hydrochloride

There total 8 articles about Thr(CH2Ph)-Dopa(diCH2Ph)-Lys2(Cl)> p-nitrophenyl ester hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 111104-10-0
Boc-Thr(CH2Ph)-Dopa(diCH2Ph)-Lys2(Cl)> p-nitrophenyl ester

: 111122-60-2
Thr(CH2Ph)-Dopa(diCH2Ph)-Lys2(Cl)> p-nitrophenyl ester hydrochloride

Guidance literature:: With hydrogenchloride; Yield given. Multistep reaction; 1.) dioxane, RT, 1 h; 2.) ether, dioxane, RT, 2 h, overnight, refrigerator;

Reference yield:

: 15260-10-3
N-(t-Butyloxycarbonyl)-O-(phenylmethyl)-L-threonine

: 111122-60-2
Thr(CH2Ph)-Dopa(diCH2Ph)-Lys2(Cl)> p-nitrophenyl ester hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) N-methylmorpholine; 2.) DCCI / 2.) chloroform; 3.) chloroform, 0 deg C, 2 h, 5 deg C, overnight

2: 1.) 0.7 M HCl / 1.) dioxane, RT, 1 h; 2.) ether, dioxane, RT, 2 h, overnight, refrigerator

With 4-methyl-morpholine; hydrogenchloride; dicyclohexyl-carbodiimide;

Reference yield:

: 59727-98-9
3-[3,4-di(benzyloxy)phenyl]-2-{[(tert-butoxy)carbonyl]amino}propanoic acid

: 111122-60-2
Thr(CH2Ph)-Dopa(diCH2Ph)-Lys2(Cl)> p-nitrophenyl ester hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) N-methylmorpholine; 2.) DCCI / 2.) chloroform; 3.) chloroform, 0 deg C, 2 h, 5 deg C, overnight

2: 1.) 1.1 M HCl / 1.) dioxane, RT, 1 h; 2.) ether, dioxane, RT, 2 h, overnight, refrigerator

3: 1.) N-methylmorpholine; 2.) DCCI / 2.) chloroform; 3.) chloroform, 0 deg C, 2 h, 5 deg C, overnight

4: 1.) 0.7 M HCl / 1.) dioxane, RT, 1 h; 2.) ether, dioxane, RT, 2 h, overnight, refrigerator

With 4-methyl-morpholine; hydrogenchloride; dicyclohexyl-carbodiimide;