1,1'-(1,4-Phenylenedicyclohexylidene)bis

Base Information

• Chemical Name: 1,1'-(1,4-Phenylenedicyclohexylidene)bis
• CAS No.: 76916-13-7
• Molecular Formula: C₂₈H₄₄N₂
• Molecular Weight: 408.671
• Mol file: 76916-13-7.mol

Synonyms:

Chemical Property of 1,1'-(1,4-Phenylenedicyclohexylidene)bis

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1,1'-(1,4-Phenylenedicyclohexylidene)bis

There total 3 articles about 1,1'-(1,4-Phenylenedicyclohexylidene)bis which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-piperidinocyclohexylcarbonitrile (3867-15-0) + 1.4-dibromobenzene (106-37-6) → 4-Bromophencyclidine (2201-33-4) + 1,1'-(1,4-Phenylenedicyclohexylidene)bis (76916-13-7)

Guidance literature:

With magnesium; Yield given. Multistep reaction; 1.) benzene, ether, 2.) reflux, 4 h;

DOI:10.1021/jo00323a014

Reference yield:

1-piperidinocyclohexylcarbonitrile (3867-15-0) + 1.4-dibromobenzene (106-37-6) → 1,1'-(1,4-Phenylenedicyclohexylidene)bis (76916-13-7)

Guidance literature:

With magnesium; Yield given. Multistep reaction; 1.) Et₂O, THF, reflux, 5 h; 2.) THF, Et₂O, reflux, 1 h;

DOI:10.1021/jo00329a037

Reference yield:

1-piperidinocyclohexylcarbonitrile (3867-15-0) + para-diiodobenzene (624-38-4,1032416-46-8) → 4-iodophencyclidine (77415-80-6) + 1-<1-(1,1'-Biphenyl-4-yl)cyclohexyl>piperidine (77415-81-7) + 1,1'-(1,4-Phenylenedicyclohexylidene)bis (76916-13-7)

Guidance literature:

With magnesium; Yield given. Multistep reaction. Yields of byproduct given; 1.) ether, benzene, reflux, 2.) reflux, 4 h;

DOI:10.1021/jo00326a033

upstream raw materials:

1-piperidinocyclohexylcarbonitrile

1.4-dibromobenzene

para-diiodobenzene