2-naphthylcarbonyl-Val-Phe-Pro-Gly-{1-[(S)-2-amino-3-phenylpropyl]-3-(2-oxoethyl)-3H-imidazol-1-ium}-Val-NH₂ trifluoroacetate

Base Information

• Chemical Name: 2-naphthylcarbonyl-Val-Phe-Pro-Gly-{1-[(S)-2-amino-3-phenylpropyl]-3-(2-oxoethyl)-3H-imidazol-1-ium}-Val-NH₂ trifluoroacetate
• CAS No.: 1067879-09-7
• Molecular Formula: C₂F₃O₂*C₅₁H₆₂N₉O₇
• Molecular Weight: 1026.13

Synonyms:

Chemical Property of 2-naphthylcarbonyl-Val-Phe-Pro-Gly-{1-[(S)-2-amino-3-phenylpropyl]-3-(2-oxoethyl)-3H-imidazol-1-ium}-Val-NH₂ trifluoroacetate

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Technology Process of 2-naphthylcarbonyl-Val-Phe-Pro-Gly-{1-[(S)-2-amino-3-phenylpropyl]-3-(2-oxoethyl)-3H-imidazol-1-ium}-Val-NH₂ trifluoroacetate

There total 1 articles about 2-naphthylcarbonyl-Val-Phe-Pro-Gly-{1-[(S)-2-amino-3-phenylpropyl]-3-(2-oxoethyl)-3H-imidazol-1-ium}-Val-NH₂ trifluoroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-[(S)-2-azido-3-phenylpropyl]-3-[(S)-1-carboxy-3-methylbutyl]-3H-imidazol-1-ium trifluoroacetate (1067878-98-1) + N-(fluoren-9-ylmethoxycarbonyl)glycine (29022-11-5) + Fmoc-Val-OH (68858-20-8) + Fmoc-Pro-OH (71989-31-6) + N-Fmoc L-Phe (35661-40-6) + trifluoroacetic acid (76-05-1) + naphthalene-2-carboxylate (93-09-4) → 2-naphthylcarbonyl-Val-Phe-Pro-Gly-{1-[(S)-2-amino-3-phenylpropyl]-3-(2-oxoethyl)-3H-imidazol-1-ium}-Val-NH2 trifluoroacetate (1067879-09-7)

Guidance literature:

Fmoc-Val-OH; With N-ethylmorpholine;; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; In N,N-dimethyl-formamide; for 2h; solid phase reaction;

With piperidine; In N,N-dimethyl-formamide; solid phase reaction;

1-[(S)-2-azido-3-phenylpropyl]-3-[(S)-1-carboxy-3-methylbutyl]-3H-imidazol-1-ium trifluoroacetate; N-(fluoren-9-ylmethoxycarbonyl)glycine; Fmoc-Val-OH; Fmoc-Pro-OH; N-Fmoc L-Phe; trifluoroacetic acid; naphthalene-2-carboxylate; Further stages;

DOI:10.1002/ejoc.200800234

upstream raw materials:

1-[(S)-2-azido-3-phenylpropyl]-3-[(S)-1-carboxy-3-methylbutyl]-3H-imidazol-1-ium trifluoroacetate

N-(fluoren-9-ylmethoxycarbonyl)glycine

Fmoc-Val-OH

Fmoc-Pro-OH

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