(5R)-8c-hydroxy-7t-hydroxymethyl-5r-(3,4,5-trimethoxy-phenyl)-5,6,7,8-tetrahydro-naphtho[2,3-d][1,3]dioxole-6c-carboxylic acid-(N'-cyclohexyl-hydrazide)

Base Information

Chemical Name:(5R)-8c-hydroxy-7t-hydroxymethyl-5r-(3,4,5-trimethoxy-phenyl)-5,6,7,8-tetrahydro-naphtho[2,3-d][1,3]dioxole-6c-carboxylic acid-(N'-cyclohexyl-hydrazide)
CAS No.:102380-51-8
Molecular Formula:C₂₈H₃₆N₂O₈
Molecular Weight:528.602
Hs Code.:

(5<i>R</i>)-8<i>c</i>-hydroxy-7<i>t</i>-hydroxymethyl-5<i>r</i>-(3,4,5-trimethoxy-phenyl)-5,6,7,8-tetrahydro-naphtho[2,3-<i>d</i>][1,3]dioxole-6<i>c</i>-carboxylic acid-(<i>N</i>'-cyclohexyl-hydrazide)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (5R)-8c-hydroxy-7t-hydroxymethyl-5r-(3,4,5-trimethoxy-phenyl)-5,6,7,8-tetrahydro-naphtho[2,3-d][1,3]dioxole-6c-carboxylic acid-(N'-cyclohexyl-hydrazide)

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Technology Process of (5R)-8c-hydroxy-7t-hydroxymethyl-5r-(3,4,5-trimethoxy-phenyl)-5,6,7,8-tetrahydro-naphtho[2,3-d][1,3]dioxole-6c-carboxylic acid-(N'-cyclohexyl-hydrazide)

There total 3 articles about (5R)-8c-hydroxy-7t-hydroxymethyl-5r-(3,4,5-trimethoxy-phenyl)-5,6,7,8-tetrahydro-naphtho[2,3-d][1,3]dioxole-6c-carboxylic acid-(N'-cyclohexyl-hydrazide) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 124245-73-4,124338-42-7
podophyllinic acid cyclohexyLiDenehydrazide

: 102380-51-8
(5R)-8c-hydroxy-7t-hydroxymethyl-5r-(3,4,5-trimethoxy-phenyl)-5,6,7,8-tetrahydro-naphtho[2,3-d][1,3]dioxole-6c-carboxylic acid-(N'-cyclohexyl-hydrazide)

Guidance literature:: With ethanol; nickel; Hydrogenation;
DOI:10.1002/hlca.19590420334

Reference yield:

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 102380-51-8
(5R)-8c-hydroxy-7t-hydroxymethyl-5r-(3,4,5-trimethoxy-phenyl)-5,6,7,8-tetrahydro-naphtho[2,3-d][1,3]dioxole-6c-carboxylic acid-(N'-cyclohexyl-hydrazide)

Guidance literature:: Multi-step reaction with 2 steps

1: benzene

2: Raney nickel; aqueous ethanol / Hydrogenation

With ethanol; nickel; benzene;
DOI:10.1002/hlca.19590420334

Reference yield:

: 78178-41-3
podophyllinic acid hydrazide

: 102380-51-8
(5R)-8c-hydroxy-7t-hydroxymethyl-5r-(3,4,5-trimethoxy-phenyl)-5,6,7,8-tetrahydro-naphtho[2,3-d][1,3]dioxole-6c-carboxylic acid-(N'-cyclohexyl-hydrazide)

Guidance literature:: Multi-step reaction with 2 steps

1: benzene

2: Raney nickel; aqueous ethanol / Hydrogenation

With ethanol; nickel; benzene;
DOI:10.1002/hlca.19590420334