bis(2,6-diisopropylphenolato)zirconium dichloride bis(tetrahydrofuran)

Base Information

Chemical Name:bis(2,6-diisopropylphenolato)zirconium dichloride bis(tetrahydrofuran)
CAS No.:1355163-35-7
Molecular Formula:C₃₂H₅₀Cl₂O₄Zr
Molecular Weight:660.877
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Chemical Property of bis(2,6-diisopropylphenolato)zirconium dichloride bis(tetrahydrofuran)

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Technology Process of bis(2,6-diisopropylphenolato)zirconium dichloride bis(tetrahydrofuran)

There total 1 articles about bis(2,6-diisopropylphenolato)zirconium dichloride bis(tetrahydrofuran) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 11.0%

: 109-99-9,24979-97-3,77392-70-2
tetrahydrofuran

: 72727-49-2
lithium 2,6-diisopropylphenolate

: 10026-11-6
zirconium(IV) chloride

: 1355163-35-7
bis(2,6-diisopropylphenolato)zirconium dichloride bis(tetrahydrofuran)

Guidance literature:: In tetrahydrofuran; diethyl ether; THF added to ZrCl4 (10.6 mmol), stirred for 1 h, evapd., suspnd. in Et2O, cooled to -78°C, Et2O soln. of Li compd. added, mixt. stirred for 20 h; filtered, crystd. on storage at -30°C, elem. anal.;
DOI:10.1002/ejic.201100548