N,3-dimethyl-N′-methylenebenzohydrazide

Base Information

• Chemical Name: N,3-dimethyl-N′-methylenebenzohydrazide
• CAS No.: 1427283-30-4
• Molecular Formula: C₁₀H₁₂N₂O
• Molecular Weight: 176.218
• Mol file: 1427283-30-4.mol

Synonyms:

Chemical Property of N,3-dimethyl-N′-methylenebenzohydrazide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N,3-dimethyl-N′-methylenebenzohydrazide

There total 2 articles about N,3-dimethyl-N′-methylenebenzohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-Methylbenzoyl chloride (1711-06-4) → N,3-dimethyl-N′-methylenebenzohydrazide (1427283-30-4)

Guidance literature:

Multi-step reaction with 2 steps

1: chloroform / 20 °C / Schlenk technique; Inert atmosphere

2: toluene / Schlenk technique; Inert atmosphere; Reflux

In chloroform; toluene;

DOI:10.1039/c3ob40195b

Reference yield:

formaldehyd (50-00-0,30525-89-4,61233-19-0) + C9H12N2O → N,3-dimethyl-N′-methylenebenzohydrazide (1427283-30-4)

Guidance literature:

In toluene; Schlenk technique; Inert atmosphere; Reflux;

DOI:10.1039/c3ob40195b

upstream raw materials:

3-Methylbenzoyl chloride

formaldehyd