C₄₇H₆₃N₉O₁₀S

Base Information

• Chemical Name: C₄₇H₆₃N₉O₁₀S
• CAS No.: 222640-07-5
• Molecular Formula: C₄₇H₆₃N₉O₁₀S
• Molecular Weight: 946.138
• Mol file: 222640-07-5.mol

Synonyms:

Chemical Property of C₄₇H₆₃N₉O₁₀S

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₄₇H₆₃N₉O₁₀S

There total 6 articles about C₄₇H₆₃N₉O₁₀S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-(2-amino-ethyl)-benzenesulfonamide; hydrochloride (53672-99-4) → C47H63N9O10S (222640-07-5)

Guidance literature:

Multi-step reaction with 5 steps

1: BOP; HOBt; NMM

2: 4 N aq. HCl

3: BOP; HOBt; NMM

4: 4 N aq. HCl

5: BOP; HOBt; NMM

With 4-methyl-morpholine; hydrogenchloride; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; benzotriazol-1-ol; 1: Condensation / 2: Hydrolysis / 3: Condensation / 4: Hydrolysis / 5: Condensation;

DOI:10.1016/S0960-894X(99)00443-6

Reference yield:

3(S)-(N-tert-butoxycarbonylamino)-2(R,S)-hydroxy-4-phenylbutyric acid (191849-93-1) → C47H63N9O10S (222640-07-5)

Guidance literature:

Multi-step reaction with 5 steps

1: BOP; HOBt; NMM

2: 4 N aq. HCl

3: BOP; HOBt; NMM

4: 4 N aq. HCl

5: BOP; HOBt; NMM

With 4-methyl-morpholine; hydrogenchloride; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; benzotriazol-1-ol; 1: Condensation / 2: Hydrolysis / 3: Condensation / 4: Hydrolysis / 5: Condensation;

DOI:10.1016/S0960-894X(99)00443-6

Reference yield:

tert-butyl (2-(phenylsulfonamido)ethyl)carbamate (222639-98-7) → C47H63N9O10S (222640-07-5)

Guidance literature:

Multi-step reaction with 6 steps

1: 4 N aq. HCl

2: BOP; HOBt; NMM

3: 4 N aq. HCl

4: BOP; HOBt; NMM

5: 4 N aq. HCl

6: BOP; HOBt; NMM

With 4-methyl-morpholine; hydrogenchloride; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; benzotriazol-1-ol; 1: Hydrolysis / 2: Condensation / 3: Hydrolysis / 4: Condensation / 5: Hydrolysis / 6: Condensation;

DOI:10.1016/S0960-894X(99)00443-6

upstream raw materials:

N-(2-amino-ethyl)-benzenesulfonamide; hydrochloride

3(S)-(N-tert-butoxycarbonylamino)-2(R,S)-hydroxy-4-phenylbutyric acid

tert-butyl (2-(phenylsulfonamido)ethyl)carbamate

[2-(2-benzenesulfonylamino-ethylcarbamoyl)-1-benzyl-2-hydroxy-ethyl]-carbamic acid tert-butyl ester