2,3-dianil of 3-phenyl-2,3-dioxopropionanilide

Base Information

• Chemical Name: 2,3-dianil of 3-phenyl-2,3-dioxopropionanilide
• CAS No.: 80056-94-6
• Molecular Formula: C₂₇H₂₁N₃O
• Molecular Weight: 403.483
• Mol file: 80056-94-6.mol

Synonyms:

Chemical Property of 2,3-dianil of 3-phenyl-2,3-dioxopropionanilide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,3-dianil of 3-phenyl-2,3-dioxopropionanilide

There total 2 articles about 2,3-dianil of 3-phenyl-2,3-dioxopropionanilide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

β-anilino-cinnamic acid anilide (52561-86-1) + Nitrosobenzene (586-96-9) → 2,3-dianil of 3-phenyl-2,3-dioxopropionanilide (80056-94-6)

Guidance literature:

With sodium hydroxide; ethanol; In ethanol; Heating;

DOI:10.1007/BF00900006

Reference yield:

3-phenyl-3-phenylimino-propionanilide (3422-79-5) + Nitrosobenzene (586-96-9) → 2,3-dianil of 3-phenyl-2,3-dioxopropionanilide (80056-94-6)

Guidance literature:

With triethylamine; In acetonitrile; at 29.9 ℃; Thermodynamic data; Kinetics; Mechanism; further temp.; ΔH(excit.), ΔS(excit.);

Reference yield: 57.0%

phenyl isocyanate (103-71-9) + 2,3-dianil of 3-phenyl-2,3-dioxopropionanilide (80056-94-6) → 1,3,4-Triphenyl-5-[(Z)-phenylimino]-imidazolidin-2-one (80858-25-9)

Guidance literature:

In benzene; Mechanism; Heating;

DOI:10.1007/BF00900006

upstream raw materials:

β-anilino-cinnamic acid anilide

Nitrosobenzene

3-phenyl-3-phenylimino-propionanilide

Downstream raw materials:

1,3,4-Triphenyl-5-[(Z)-phenylimino]-imidazolidin-2-one