Co(4,4'-(hexafluoroisopropylidene)bis(benzoic acid)^(2-))(2,5-bis(4-pyridyl)-1,3,4-thiadiazole)*dimethylformamide

Base Information

• Chemical Name: Co(4,4'-(hexafluoroisopropylidene)bis(benzoic acid)^(2-))(2,5-bis(4-pyridyl)-1,3,4-thiadiazole)*dimethylformamide
• CAS No.: 1353387-20-8
• Molecular Formula: C₃H₇NO*C₁₂H₈N₄S*C₁₇H₈F₆O₄*Co
• Molecular Weight: 762.615
• Mol file: 1353387-20-8.mol

Synonyms:

Chemical Property of Co(4,4'-(hexafluoroisopropylidene)bis(benzoic acid)^(2-))(2,5-bis(4-pyridyl)-1,3,4-thiadiazole)*dimethylformamide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of Co(4,4'-(hexafluoroisopropylidene)bis(benzoic acid)^(2-))(2,5-bis(4-pyridyl)-1,3,4-thiadiazole)*dimethylformamide

There total 1 articles about Co(4,4'-(hexafluoroisopropylidene)bis(benzoic acid)^(2-))(2,5-bis(4-pyridyl)-1,3,4-thiadiazole)*dimethylformamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

cobalt(II) nitrate tetrahydrate + 2,5-bis(4-pyridyl)-1,3,4-thiadiazole (15311-09-8) + 2,2-bis(4-carboxyphenyl)hexafluoropropane (1171-47-7,936941-90-1) + N,N-dimethyl-formamide (68-12-2,33513-42-7) → Co(4,4'-(hexafluoroisopropylidene)bis(benzoic acid)(2-))(2,5-bis(4-pyridyl)-1,3,4-thiadiazole)*dimethylformamide (1353387-20-8)

Guidance literature:

With NaOH; In water; N,N-dimethyl-formamide; to benzoic-compd. and diazole-compd. in DMF Co-compd. in H2O added at 30°C, pH ajusted to 5.5 with aq. NaOH, kept at 160°C for 96 h; elem. anal.;

DOI:10.1080/15533174.2011.591876

upstream raw materials:

2,5-bis(4-pyridyl)-1,3,4-thiadiazole

2,2-bis(4-carboxyphenyl)hexafluoropropane

N,N-dimethyl-formamide

Refernces