bis(cis-bis(diphenylphosphino)ethylene)gold(I) hexafluorophosphate

Base Information

Chemical Name:bis(cis-bis(diphenylphosphino)ethylene)gold(I) hexafluorophosphate
CAS No.:129596-70-9
Molecular Formula:C₅₂H₄₄AuP₄*F₆P
Molecular Weight:1134.75
Hs Code.:

Synonyms:

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Chemical Property of bis(cis-bis(diphenylphosphino)ethylene)gold(I) hexafluorophosphate

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Technology Process of bis(cis-bis(diphenylphosphino)ethylene)gold(I) hexafluorophosphate

There total 2 articles about bis(cis-bis(diphenylphosphino)ethylene)gold(I) hexafluorophosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: ammonium hexafluorophosphate

: sodium tetrachloroaurate(III)*0.5H₂O

: 983-80-2
cis-1,2-bis-(diphenylphosphino)ethene

: 129596-70-9
bis(cis-bis(diphenylphosphino)ethylene)gold(I) hexafluorophosphate

Guidance literature:: With thiodiglycol; In water; acetone; soln. of Au-complex and NH4PF6 in H2O, redn. by addn. of thiodiglycol in acetone, addn. of Au-soln. to a warm soln. of phosphine-compd. in acetone; rotary evapn., recrystn. from CH3CN; elem. anal.;

Reference yield:

: 129499-98-5
[Au(tht)₂]PF₆

: 983-80-2
cis-1,2-bis-(diphenylphosphino)ethene

: 129596-70-9
bis(cis-bis(diphenylphosphino)ethylene)gold(I) hexafluorophosphate

: [Au2(μ-cis-1,2-bis(diphenylphosphino)ethylene)2](PF6)2

Guidance literature:: In dichloromethane; addn. of ligand to a soln. of Au complex in CH2Cl2 at room temp., stirring for 30 min; filtration through Celite, concn. in vac., addn. of ether, obtained as amixt., not sepd.;
DOI:10.1039/c2dt11722c

Reference yield:

: 129596-70-9
bis(cis-bis(diphenylphosphino)ethylene)gold(I) hexafluorophosphate

: 932-72-9
(Dichloroiodo)benzene

: [Au2(μ-cis-1,2-bis(diphenylphosphino)ethylene)2](PF6)2

: 64645-30-3
(AuCl)2(μ-cis-1,2-bis(diphenylphosphino)ethylene)

: 1370451-58-3
[AuCl₂(cis-1,2-bis(diphenylphosphino)ethylene)]PF₆

Guidance literature:: In dichloromethane; addn. of a soln. of C6H5ICl2 in CH2Cl2 to a soln. of a mixt. of Au complexes in CH2Cl2 at room temp., stirring for 1 h in the dark; evapn. in vac., addn. of ether, filtration, washing ppt. with ether, drying; obtained as a mixt., not sepd.;
DOI:10.1039/c2dt11722c