1-Benzyl-2-hydrazinyl-1H-benzo[d]imidazole

Base Information

• Chemical Name: 1-Benzyl-2-hydrazinyl-1H-benzo[d]imidazole
• CAS No.: 14180-45-1
• Molecular Formula: C14H14N4
• Molecular Weight: 238.292
• DSSTox Substance ID: DTXSID30399090
• Wikidata: Q82201438
• Mol file: 14180-45-1.mol

Synonyms:14180-45-1;1-Benzyl-2-hydrazinyl-1H-benzo[d]imidazole;(1-benzylbenzimidazol-2-yl)hydrazine;Oprea1_204274;1-benzyl-2-hydrazinobenzimidazole;DTXSID30399090;AKOS002664712;1-Benzyl-2-hydrazino-1H-benzimidazole;1-benzyl-2-hydrazinyl-1H-1,3-benzodiazole

Chemical Property of 1-Benzyl-2-hydrazinyl-1H-benzo[d]imidazole

Chemical Property:

• PSA: 55.87000
• LogP: 3.14350
• XLogP3: 2.6
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 3
• Exact Mass: 238.121846464
• Heavy Atom Count: 18
• Complexity: 265

Purity/Quality:

99% ^*data from raw suppliers

1-Benzyl-2-hydrazinyl-1H-benzo[d]imidazole 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C(C=C1)CN2C3=CC=CC=C3N=C2NN

Technology Process of 1-Benzyl-2-hydrazinyl-1H-benzo[d]imidazole

There total 2 articles about 1-Benzyl-2-hydrazinyl-1H-benzo[d]imidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-benzyl-2-chlorobenzimidazole (43181-78-8) → (1-benzyl-2-benzimidazolyl)hydrazine (14180-45-1)

Guidance literature:

With hydrazine hydrate; at 160 ℃; for 5h;

DOI:10.1016/j.ejmech.2009.11.031

Reference yield:

→ (1-benzyl-2-benzimidazolyl)hydrazine (14180-45-1)

Guidance literature:

2-Chlor-1-benzyl-benzimidazol, N2H4*H2O, im Rohr (4h, 150-155grad);

Reference yield: 93.0%

ferrocenecarboxaldehyde (12093-10-6) + (1-benzyl-2-benzimidazolyl)hydrazine (14180-45-1) → C10H9FeCHNNHC7H4N2CH2C6H5

Guidance literature:

In ethanol; boiling;

upstream raw materials:

1-benzyl-2-chlorobenzimidazole

Downstream raw materials:

1-benzothiazol-2-yl-5-(1-benzyl-1H-benzoimidazol-2-yl)-3-methyl-formazan

1-benzothiazol-2-yl-5-(1-benzyl-1H-benzoimidazol-2-yl)-3-methyl-formazan

1-benzooxazol-2-yl-5-(1-benzyl-1H-benzoimidazol-2-yl)-3-methyl-formazan

C₂₁H₁₉N₅S