4-hexyl-2,5-dihydroxy-benzaldehyde

Base Information

• Chemical Name: 4-hexyl-2,5-dihydroxy-benzaldehyde
• CAS No.: 858250-53-0
• Molecular Formula: C₁₃H₁₈O₃
• Molecular Weight: 222.284
• Mol file: 858250-53-0.mol

Synonyms:

Chemical Property of 4-hexyl-2,5-dihydroxy-benzaldehyde

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4-hexyl-2,5-dihydroxy-benzaldehyde

There total 4 articles about 4-hexyl-2,5-dihydroxy-benzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-hexylphenol (3226-32-2) → 4-hexyl-2,5-dihydroxy-benzaldehyde (858250-53-0)

Guidance literature:

Multi-step reaction with 4 steps

1: aqueous NaOH; K₂S₂O₈ / <40 / Erwaermen des Reaktionsprodukts mit konz. wss. HCl auf 70grad

2: potassium hydrogencarbonate; glycerol; carbon dioxide / 130 °C / Behandeln des Reaktionsprodukts mit Acetanhydrid und Pyridin

3: phosphorus (V)-chloride

With sodium hydroxide; dipotassium peroxodisulfate; carbon dioxide; phosphorus pentachloride; potassium hydrogencarbonate; glycerol;

DOI:10.1002/hlca.19470300116

Reference yield:

2-hexylhydroquinone (4197-72-2) → 4-hexyl-2,5-dihydroxy-benzaldehyde (858250-53-0)

Guidance literature:

Multi-step reaction with 3 steps

1: potassium hydrogencarbonate; glycerol; carbon dioxide / 130 °C / Behandeln des Reaktionsprodukts mit Acetanhydrid und Pyridin

2: phosphorus (V)-chloride

With carbon dioxide; phosphorus pentachloride; potassium hydrogencarbonate; glycerol;

DOI:10.1002/hlca.19470300116

Reference yield:

2,5-diacetoxy-4-hexyl-benzoic acid → 4-hexyl-2,5-dihydroxy-benzaldehyde (858250-53-0)

Guidance literature:

Multi-step reaction with 2 steps

1: phosphorus (V)-chloride

With phosphorus pentachloride;

DOI:10.1002/hlca.19470300116

upstream raw materials:

2-hexylphenol

2-hexylhydroquinone