2,7-dimethyldibenzo<1,2>diazepin-11-one

Base Information

• Chemical Name: 2,7-dimethyldibenzo<1,2>diazepin-11-one
• CAS No.: 87775-52-8
• Molecular Formula: C₁₅H₁₂N₂O
• Molecular Weight: 236.273

Synonyms:

Chemical Property of 2,7-dimethyldibenzo<1,2>diazepin-11-one

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of 2,7-dimethyldibenzo<1,2>diazepin-11-one

There total 3 articles about 2,7-dimethyldibenzo<1,2>diazepin-11-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.5%

5,3'-dimethyl-2,2'-dinitrodiphenylmethane (84797-80-8) → 2,5-dimethyl-9(10H)-acridone (87025-04-5) + 2,7-dimethyldibenzo<1,2>diazepin-11-one (87775-52-8) + 4-Hydroxy-2,7-dimethyl-dibenzo[c,f][1,2]diazepin-11-one (87775-49-3) + 5,3'-dimethyl-2,2'-dinitrobenzophenone (87775-46-0) + 2,7-dimethyldibenzo<1,2>diazepin-11-one-5-oxide (87025-01-2) + 5-methyl-3-(3'-methyl-2'-nitrophenyl)-2,1-benzisoxazole (87024-97-3)

Guidance literature:

acidic ethanol; In ethanol; for 10.5h; Product distribution; Mechanism; Irradiation;

Reference yield: 25.8%

5,3'-dimethyl-2,2'-dinitrodiphenylmethane (84797-80-8) → 2,5-dimethyl-9(10H)-acridone (87025-04-5) + 2,7-dimethyldibenzo<1,2>diazepin-11-one (87775-52-8) + 5,3'-dimethyl-2,2'-dinitrobenzophenone (87775-46-0) + 2,7-dimethyldibenzo<1,2>diazepin-11-one-5-oxide (87025-01-2)

Guidance literature:

In isopropyl alcohol; for 7h; Further byproducts given; Irradiation;

Reference yield: 4.0%

5,3'-dimethyl-2,2'-dinitrodiphenylmethane (84797-80-8) → 2,5-dimethyl-9(10H)-acridone (87025-04-5) + 2,7-dimethyldibenzo<1,2>diazepin-11-one (87775-52-8) + 5,3'-dimethyl-2,2'-dinitrobenzophenone (87775-46-0) + 2,7-dimethyldibenzo<1,2>diazepin-11-one-5-oxide (87025-01-2) + 5-methyl-3-(3'-methyl-2'-nitrophenyl)-2,1-benzisoxazole (87024-97-3)

Guidance literature:

In isopropyl alcohol; for 7h; Product distribution; Mechanism; Irradiation;

upstream raw materials:

5,3'-dimethyl-2,2'-dinitrodiphenylmethane

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