dicyclohexyl-amine; formate

Base Information

• Chemical Name: dicyclohexyl-amine; formate
• CAS No.: 132001-45-7
• Molecular Formula: CH₂O₂*C₁₂H₂₃N
• Molecular Weight: 227.347
• Mol file: 132001-45-7.mol

Synonyms:

Chemical Property of dicyclohexyl-amine; formate

Chemical Property:

Purity/Quality:

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Technology Process of dicyclohexyl-amine; formate

There total 1 articles about dicyclohexyl-amine; formate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 13.0%

carbon dioxide (124-38-9,18923-20-1) + N-cyclohexyl-cyclohexanamine (101-83-7) → dicyclohexyl-amine; formate (132001-45-7)

Guidance literature:

With [Re(Br)(H)(NO)(PiPr₃)2]; tris(pentafluorophenyl)borate; hydrogen; In tetrahydrofuran; at 80 ℃; for 34h; Time; Catalytic behavior; Autoclave;

DOI:10.1021/ja402381d

upstream raw materials:

carbon dioxide

N-cyclohexyl-cyclohexanamine