{(tetraphenylporphinato)Rh(n-hexyl)}

Base Information

Chemical Name:{(tetraphenylporphinato)Rh(n-hexyl)}
CAS No.:106799-98-8
Molecular Formula:C₅₀H₄₁N₄Rh
Molecular Weight:800.808
Hs Code.:

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Chemical Property of {(tetraphenylporphinato)Rh(n-hexyl)}

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Technology Process of {(tetraphenylporphinato)Rh(n-hexyl)}

There total 2 articles about {(tetraphenylporphinato)Rh(n-hexyl)} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 51669-90-0
{(tetraphenylporphinato)Rh(dimethylamine)2}Cl

: 629-05-0
n-octyne

: 106799-98-8
{(tetraphenylporphinato)Rh(n-hexyl)}

Guidance literature:: In tetrahydrofuran; Electrolysis; controlled potential electrolysis at -1.10 V vs. SCE in the presence of 0.2 M tetra-n-butylammonium perchlorate under inert atmosphere, after the current reached background level soln. was transferred to another flask and kept for 40 min at room temp.; soln. was evapd., extd. with benzene at 10°C, ext. chromd. on a SiO2 column under inert atmosphere (eluent benzene);

Reference yield:

: 51669-90-0
{(tetraphenylporphinato)Rh(dimethylamine)2}Cl

: 111-66-0,25068-25-1
oct-1-ene

: 106799-98-8
{(tetraphenylporphinato)Rh(n-hexyl)}

Guidance literature:: In tetrahydrofuran; Electrolysis; controlled potential electrolysis at -1.10 V vs. SCE in the presence of 0.2 M tetra-n-butylammonium perchlorate under inert atmosphere for 480 s; not isolated; reaction monitored by UV spectroscopy;