(1'RS,1''Z,2SR,2'E,3SR)-2-<5''-(1''',3'''-dioxan-2'''-yl)-3''-oxopent-1''-enyl>-3-<3'-(diphenylphosphinoyl)-1'-methylprop-2'-enyl>-2-methylcyclopentanone

Base Information

Chemical Name:(1'RS,1''Z,2SR,2'E,3SR)-2-<5''-(1''',3'''-dioxan-2'''-yl)-3''-oxopent-1''-enyl>-3-<3'-(diphenylphosphinoyl)-1'-methylprop-2'-enyl>-2-methylcyclopentanone
CAS No.:122406-52-4
Molecular Formula:C₃₁H₃₇O₅P
Molecular Weight:520.606
Hs Code.:

Synonyms:

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Chemical Property of (1'RS,1''Z,2SR,2'E,3SR)-2-<5''-(1''',3'''-dioxan-2'''-yl)-3''-oxopent-1''-enyl>-3-<3'-(diphenylphosphinoyl)-1'-methylprop-2'-enyl>-2-methylcyclopentanone

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Technology Process of (1'RS,1''Z,2SR,2'E,3SR)-2-<5''-(1''',3'''-dioxan-2'''-yl)-3''-oxopent-1''-enyl>-3-<3'-(diphenylphosphinoyl)-1'-methylprop-2'-enyl>-2-methylcyclopentanone

There total 2 articles about (1'RS,1''Z,2SR,2'E,3SR)-2-<5''-(1''',3'''-dioxan-2'''-yl)-3''-oxopent-1''-enyl>-3-<3'-(diphenylphosphinoyl)-1'-methylprop-2'-enyl>-2-methylcyclopentanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1120-73-6
2-methyl-2-cyclopenten-1-one

: 17668-60-9
trans-crotyldiphenylphosphine oxide

: 108662-09-5
(Z)-5-(1',3'-dioxan-2'-yl)-1-(phenylsulfonyl)pent-1-en-3-one

: 122406-52-4
(1'RS,1''Z,2SR,2'E,3SR)-2-<5''-(1''',3'''-dioxan-2'''-yl)-3''-oxopent-1''-enyl>-3-<3'-(diphenylphosphinoyl)-1'-methylprop-2'-enyl>-2-methylcyclopentanone

: 122406-51-3
(1'RS,1''E,2SR,2'E,3SR)-2-<5''-(1''',3'''-dioxan-2'''-yl)-3''-oxopent-1''-enyl>-3-<3'-(diphenylphosphinoyl)-1'-methylprop-2'-enyl>-2-methylcyclopentanone

Guidance literature:: With n-butyllithium; Yield given. Multistep reaction. Yields of byproduct given; 1.) THF, hexane, -60 deg C, 10 min, 2.) -20 deg C to -15 deg C, 5 min;
DOI:10.1021/jo00282a038

Reference yield:

: 1120-73-6
2-methyl-2-cyclopenten-1-one

: 17668-60-9
trans-crotyldiphenylphosphine oxide

: 108643-98-7
(E)-5-(1',3'-dioxan-2'-yl)-1-(phenylsulfonyl)pent-1-en-3-one

: 122406-52-4
(1'RS,1''Z,2SR,2'E,3SR)-2-<5''-(1''',3'''-dioxan-2'''-yl)-3''-oxopent-1''-enyl>-3-<3'-(diphenylphosphinoyl)-1'-methylprop-2'-enyl>-2-methylcyclopentanone

: 122406-51-3
(1'RS,1''E,2SR,2'E,3SR)-2-<5''-(1''',3'''-dioxan-2'''-yl)-3''-oxopent-1''-enyl>-3-<3'-(diphenylphosphinoyl)-1'-methylprop-2'-enyl>-2-methylcyclopentanone

Guidance literature:: With n-butyllithium; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts; 1.) THF, hexane, -60 deg C, 10 min, 2.) -20 deg C to -15 deg C, 5 min;
DOI:10.1021/jo00282a038