p-tolyl-glyoxylohydroximic acid

Base Information

• Chemical Name: p-tolyl-glyoxylohydroximic acid
• CAS No.: 861366-07-6
• Molecular Formula: C₉H₉NO₃
• Molecular Weight: 179.175
• Mol file: 861366-07-6.mol

Synonyms:

Chemical Property of p-tolyl-glyoxylohydroximic acid

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of p-tolyl-glyoxylohydroximic acid

There total 1 articles about p-tolyl-glyoxylohydroximic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-methylphenylglyoxal (1075-47-4) + piloty's acid (599-71-3) → p-tolyl-glyoxylohydroximic acid (861366-07-6)

Guidance literature:

With sodium hydroxide;

DOI:10.1672/0277-5212(2001)021[0210:ACSONA]2.0.CO;2

Reference yield:

p-tolyl-glyoxylohydroximic acid (861366-07-6) → 2-hydroxyimino-2-p-tolyl-acetohydroxamic acid (861322-19-2)

Guidance literature:

With hydroxylamine hydrochloride; water; sodium acetate; α-p-tolyloxyglyoxime;

DOI:10.1672/0277-5212(2001)021[0210:ACSONA]2.0.CO;2

Reference yield:

p-tolyl-glyoxylohydroximic acid (861366-07-6) → (N-acetoxy-2-acetoxyimino-2-p-tolyl-acetimidic acid )-acetic acid-anhydride

Guidance literature:

Multi-step reaction with 2 steps

1: sodium acetate; water; hydroxylamine hydrochloride

2: sodium acetate

With hydroxylamine hydrochloride; water; sodium acetate;

upstream raw materials:

4-methylphenylglyoxal

piloty's acid

Downstream raw materials:

2-hydroxyimino-2-p-tolyl-acetohydroxamic acid