tetrabutylammonium 2,2-diphenylvinylsulphonate

Base Information

• Chemical Name: tetrabutylammonium 2,2-diphenylvinylsulphonate
• CAS No.: 114086-83-8
• Molecular Formula: C₁₄H₁₁O₃S*C₁₆H₃₆N
• Molecular Weight: 501.774
• Mol file: 114086-83-8.mol

Synonyms:

Chemical Property of tetrabutylammonium 2,2-diphenylvinylsulphonate

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of tetrabutylammonium 2,2-diphenylvinylsulphonate

There total 1 articles about tetrabutylammonium 2,2-diphenylvinylsulphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

benzophenone (119-61-9) + tetra(n-butyl)ammonium hydrogensulfate (32503-27-8) + lithium diethylphosphoryl methanesulfonate (110679-80-6) → tetrabutylammonium 2,2-diphenylvinylsulphonate (114086-83-8)

Guidance literature:

With lithium hydroxide; n-butyllithium; Yield given. Multistep reaction; 1) THF, -15 deg C, 60 min, 2) THF, -78 deg C, 30 min then RT, 18 h, 3) H₂O;

DOI:10.1016/S0040-4020(01)87688-2

upstream raw materials:

benzophenone

tetra(n-butyl)ammonium hydrogensulfate

lithium diethylphosphoryl methanesulfonate

Refernces