1,3-Dibromo-2-(methoxymethoxy)benzene

Base Information

Chemical Name:1,3-Dibromo-2-(methoxymethoxy)benzene
CAS No.:142273-81-2
Molecular Formula:C8H8Br2O2
Molecular Weight:295.958
Hs Code.:
DSSTox Substance ID:DTXSID40443215
Nikkaji Number:J1.651.646E
Wikidata:Q82260936

Synonyms:142273-81-2;1,3-dibromo-2-(methoxymethoxy)benzene;1,3-Dibromo-2-(methoxymethoxy)-benzene;Benzene, 1,3-dibromo-2-(methoxymethoxy)-;SCHEMBL5846257;DTXSID40443215;XAJIRWLAZNHZHJ-UHFFFAOYSA-N;1,3-Dibromo-2-methoxymethoxybenzene;1-Methoxymethoxy-2,6-dibromobenzene;MFCD27998238;CS-0193615;FT-0758426;E93262

Suppliers and Price of 1,3-Dibromo-2-(methoxymethoxy)benzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 6 raw suppliers

Chemical Property of 1,3-Dibromo-2-(methoxymethoxy)benzene

Chemical Property:

XLogP3:3.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:295.88706
Heavy Atom Count:12
Complexity:122

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COCOC1=C(C=CC=C1Br)Br

Technology Process of 1,3-Dibromo-2-(methoxymethoxy)benzene

There total 4 articles about 1,3-Dibromo-2-(methoxymethoxy)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 608-33-3
2,6-dibromophenol

: 107-30-2
chloromethyl methyl ether

: 142273-81-2
1,3-dibromo-2-(methoxymethoxy)benzene

Guidance literature:: With sodium hydride; In tetrahydrofuran; acetic acid methyl ester; at 0 - 20 ℃; for 2h;
DOI:10.1139/cjc-79-11-1541

Reference yield: 84.0%

: 13057-17-5
bromethyl methyl ether

: 608-33-3
2,6-dibromophenol

: 142273-81-2
1,3-dibromo-2-(methoxymethoxy)benzene

Guidance literature:: 2,6-dibromophenol; With sodium hydride; In tetrahydrofuran; mineral oil; at 0 ℃; for 0.5h;

bromethyl methyl ether; In tetrahydrofuran; mineral oil; at 20 ℃; for 3h;

Reference yield:

: 108-95-2,27073-41-2
phenol

: 142273-81-2
1,3-dibromo-2-(methoxymethoxy)benzene

Guidance literature:: Multi-step reaction with 2 steps

1: diisopropylamine; N-Bromosuccinimide / dichloromethane / 20 °C / Inert atmosphere

2: N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C / Inert atmosphere

With N-Bromosuccinimide; diisopropylamine; N-ethyl-N,N-diisopropylamine; In dichloromethane;
DOI:10.1039/c3ob41065j