2,4-dinitrophenyl ferrocenyl(methoxy)thiophosphonyl disulfide

Base Information

Chemical Name:2,4-dinitrophenyl ferrocenyl(methoxy)thiophosphonyl disulfide
CAS No.:817620-80-7
Molecular Formula:C₁₇H₁₅FeN₂O₅PS₃
Molecular Weight:510.335
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Chemical Property of 2,4-dinitrophenyl ferrocenyl(methoxy)thiophosphonyl disulfide

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Technology Process of 2,4-dinitrophenyl ferrocenyl(methoxy)thiophosphonyl disulfide

There total 1 articles about 2,4-dinitrophenyl ferrocenyl(methoxy)thiophosphonyl disulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: sodium (methoxy)ferrocenylphosphonodithioate

: 528-76-7
2,4-dinitrobenzenesulfenyl chloride

: 817620-80-7
2,4-dinitrophenyl ferrocenyl(methoxy)thiophosphonyl disulfide

Guidance literature:: In tetrahydrofuran; (N2); using Schlenk techniques; addn. of 2,4-dinitrosulfenyl chloride toflask containing NaSP(S)(OMe)Fc; addn. of THF with stirring, stirring f or 1 h; removal of solvent under reduced pressure, redissolving in CH2Cl2, filtration, concn. under vac., addn. of hexane; pptn.;
DOI:10.1039/b406007e