{oxomolybdenum(V) tetraphenylporphyrine perchlorate}

Base Information

Chemical Name:{oxomolybdenum(V) tetraphenylporphyrine perchlorate}
CAS No.:77321-00-7
Molecular Formula:C₄₄H₂₈ClMoN₄O₅
Molecular Weight:824.123
Hs Code.:

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Chemical Property of {oxomolybdenum(V) tetraphenylporphyrine perchlorate}

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Technology Process of {oxomolybdenum(V) tetraphenylporphyrine perchlorate}

There total 1 articles about {oxomolybdenum(V) tetraphenylporphyrine perchlorate} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7601-90-3
perchloric acid

: 65404-71-9
ethoxy-oxo-molybdenum(V) 5,10,15,20-tetraphenylporphyrin

: 77321-00-7
{oxomolybdenum(V) tetraphenylporphyrine perchlorate}

Guidance literature:: In perchloric acid; dichloromethane; aq. HClO4; repeated shaking of Mo-complex (in CH2Cl2) with 3% aq. HClO4; drying of org. layer (MgSO4), filtration, concn. (vac.), crystn. on layering with hexanes (4 d);

Reference yield:

: 77321-00-7
{oxomolybdenum(V) tetraphenylporphyrine perchlorate}

: 33519-60-7
(5,10,15,20-meso-tetraphenylporphyrinato)oxomolybdenum(IV)

Guidance literature:: In dichloromethane; Electrochem. Process; Controlled-potential electroreduction of Mo-complex at -0.4 V in CH2Cl2contg. 0.1 M TBAP is monitored by thin-layer UV-spectroscopy.; Spectroelectrochem. characterization of resulting compd.;