ethoxy-oxo-molybdenum(V) 5,10,15,20-tetraphenylporphyrin

Base Information

Chemical Name:ethoxy-oxo-molybdenum(V) 5,10,15,20-tetraphenylporphyrin
CAS No.:65404-71-9
Molecular Formula:C₄₆H₃₃MoN₄O₂
Molecular Weight:769.734
Hs Code.:

Synonyms:ethoxy-oxo-molybdenum(V) 5,10,15,20-tetraphenylporphyrin

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Chemical Property of ethoxy-oxo-molybdenum(V) 5,10,15,20-tetraphenylporphyrin

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Technology Process of ethoxy-oxo-molybdenum(V) 5,10,15,20-tetraphenylporphyrin

There total 5 articles about ethoxy-oxo-molybdenum(V) 5,10,15,20-tetraphenylporphyrin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 23.0%

: 917-23-7,20998-75-8
5,10,15,20-tetraphenyl-21H,23H-porphine

: 10241-05-1
molybdenum(V) chloride

: 65404-71-9
ethoxy-oxo-molybdenum(V) 5,10,15,20-tetraphenylporphyrin

Guidance literature:: With sodium acetate; In decalin; org. compd., MoCl5 and sodium acetate dissolved in decalin, soln. refluxed for 7 h at 180-190°C under N2, allowed to stand at room temp.for 12 h; filtration, dissolving of the residue in CHCl3-EtOH, filtration, evapn., dissolving in CHCl3-EtOH, chromy. (Al2O3, EtOH-CH2Cl2), recrystn. (CH2Cl2-EtOH-hexane); elem. anal.;
DOI:10.1246/bcsj.54.170

Reference yield:

: 73515-72-7
{oxomolybdenum(V) tetraphenylporphyrine(Br)}

: 65404-71-9
ethoxy-oxo-molybdenum(V) 5,10,15,20-tetraphenylporphyrin

Guidance literature:: With ethanol; In dichloromethane; addn. of ethanol to CH2Cl2 soln. of Mo complex at 25°C; monitored by UV;
DOI:10.1246/bcsj.57.194