diμ-phenoxidobis[(diethyl ether)phenylzinc(II)]

Base Information

• Chemical Name: diμ-phenoxidobis[(diethyl ether)phenylzinc(II)]
• CAS No.: 1159218-07-1
• Molecular Formula: C₃₂H₄₀O₄Zn₂
• Molecular Weight: 619.447
• Mol file: 1159218-07-1.mol

Synonyms:

Chemical Property of diμ-phenoxidobis[(diethyl ether)phenylzinc(II)]

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of diμ-phenoxidobis[(diethyl ether)phenylzinc(II)]

There total 1 articles about diμ-phenoxidobis[(diethyl ether)phenylzinc(II)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

bromobenzene (108-86-1,52753-63-6) + diethyl ether (60-29-7,927820-24-4) + oxygen (80937-33-3) + zinc(II) chloride (7646-85-7,24359-56-6) → diμ-phenoxidobis[(diethyl ether)phenylzinc(II)] (1159218-07-1)

Guidance literature:

With Mg; In diethyl ether; C6H5Br added to stirred mixt. of Mg and Et2O; stirred overnight at ambient temp.; soln. added dropwise to suspn. of ZnCl2 in Et2O at 273 K; stirred overnight; evapd., sublimated; dissolved in Et2O; stored at 238 K for 3.5 years; slowly reacted with O2;

DOI:10.1107/S0108270107057514

upstream raw materials:

bromobenzene

diethyl ether

oxygen

zinc(II) chloride