3,5-Pyridinedicarboxylic acid, 1,4-dihydro-1,2,6-trimethyl-, diethyl ester

Base Information

Chemical Name:3,5-Pyridinedicarboxylic acid, 1,4-dihydro-1,2,6-trimethyl-, diethyl ester
CAS No.:14258-07-2
Molecular Formula:C14H21NO4
Molecular Weight:267.325
Hs Code.:

Synonyms:diethyl 1,2,6-trimethyl-1,4-dihydropyridine-3,5-dicarboxylate;1,4-Dihydro-1,2,6-trimethyl-pyridin-3,5-dicarbonsaeure-diethylester;1,2,6-trimethyl-1,4-dihydro-pyridine-3,5-dicarboxylic acid diethyl ester;1,2,6-Trimethyl-3,5-diethoxycarbonyl-1,4-dihydro-pyridin;1,2,6-Trimethyl-1,4-dihydro-pyridin-3,5-dicarbonsaeure-diaethylester;N-methyl Hantzsch ester;3,5-Pyridinedicarboxylic acid,1,4-dihydro-1,2,6-trimethyl-,diethyl ester;

Suppliers and Price of 3,5-Pyridinedicarboxylic acid, 1,4-dihydro-1,2,6-trimethyl-, diethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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Total 3 raw suppliers

Chemical Property of 3,5-Pyridinedicarboxylic acid, 1,4-dihydro-1,2,6-trimethyl-, diethyl ester

Chemical Property:

PSA：55.84000
LogP:1.93400

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3,5-Pyridinedicarboxylic acid, 1,4-dihydro-1,2,6-trimethyl-, diethyl ester

There total 1 articles about 3,5-Pyridinedicarboxylic acid, 1,4-dihydro-1,2,6-trimethyl-, diethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 952-92-1
1-Benzyl-1,4-dihydronicotinamide

: 3,5-bis-ethoxycarbonyl-1,2,6-trimethyl-pyridinium; perchlorate

: 14258-07-2
1,2,6-trimethyl-1,4-dihydro-pyridine-3,5-dicarboxylic acid diethyl ester

: 15519-25-2
3-(aminocarbonyl)-1-(phenylmethyl)pyridinium perchlorate

Guidance literature:: In chloroform-d1; acetone; at 20 ℃; for 2h; Equilibrium constant;
DOI:10.1039/c39820000402

Reference yield: 67.0%

: 626-62-0
Cyclohexyl iodide

: 14258-07-2
1,2,6-trimethyl-1,4-dihydro-pyridine-3,5-dicarboxylic acid diethyl ester

: diethyl 4-cyclohexyl-1,2,6-trimethyl-1,4-dihydropyridine-3,5-dicarboxylate

Guidance literature:: With dimanganese decacarbonyl; In dichloromethane; at 20 ℃; for 12h; Inert atmosphere; Irradiation; Schlenk technique;
DOI:10.1021/acs.orglett.1c01210

Reference yield: 48.0%

: 14258-07-2
1,2,6-trimethyl-1,4-dihydro-pyridine-3,5-dicarboxylic acid diethyl ester

: 88284-48-4
2-(trimethylsilyl)phenyl trifluoromethanesulfonate

: diethyl 1,2,6-trimethyl-2-phenyl-1,2-dihydropyridine-3,5-dicarboxylate

Guidance literature:: With cesium fluoride; In acetonitrile; at 70 ℃; regioselective reaction; Inert atmosphere; Sealed tube;
DOI:10.1021/acs.orglett.7b02272