(acetone Schiff base of S-methyldithiocarbazate-H)SnPh₂Cl

Base Information

• Chemical Name: (acetone Schiff base of S-methyldithiocarbazate-H)SnPh₂Cl
• CAS No.: 1018366-74-9
• Molecular Formula: C₁₇H₁₉ClN₂S₂Sn
• Molecular Weight: 469.646
• Mol file: 1018366-74-9.mol

Synonyms:

Chemical Property of (acetone Schiff base of S-methyldithiocarbazate-H)SnPh₂Cl

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of (acetone Schiff base of S-methyldithiocarbazate-H)SnPh₂Cl

There total 1 articles about (acetone Schiff base of S-methyldithiocarbazate-H)SnPh₂Cl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Methyl 2-isopropylidenehydrazinecarbodithioate (27268-57-1) + diphenyltin(IV) dichloride (1135-99-5) → (acetone Schiff base of S-methyldithiocarbazate-H)SnPh2Cl (1018366-74-9)

Guidance literature:

In ethanol; 1 equiv. of the N-compd. in EtOH was added to boiling EtOH soln. of Ph2SnCl2, reflux for 48 h; standing overnight, ppt. was filtered off, washed with abs. EtOH, dried in vac. desiccator over anhydrous silica gel, elem. anal.;

DOI:10.1016/j.poly.2007.11.030

upstream raw materials:

Methyl 2-isopropylidenehydrazinecarbodithioate

diphenyltin(IV) dichloride

Refernces