dichloro-tetra(4-benzoyl-pyridine)nickel(II)

Base Information

• Chemical Name: dichloro-tetra(4-benzoyl-pyridine)nickel(II)
• CAS No.: 99837-09-9
• Molecular Formula: C₄₈H₃₆Cl₂N₄NiO₄
• Molecular Weight: 862.434
• Mol file: 99837-09-9.mol

Synonyms:

Chemical Property of dichloro-tetra(4-benzoyl-pyridine)nickel(II)

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of dichloro-tetra(4-benzoyl-pyridine)nickel(II)

There total 2 articles about dichloro-tetra(4-benzoyl-pyridine)nickel(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

nickel(II) chloride hexahydrate + 4-Benzoylpyridine (14548-46-0) → dichloro-tetra(4-benzoyl-pyridine)nickel(II) (99837-09-9)

Guidance literature:

In methanol; soln. of 4-Bz-Py in MeOH is added to a soln. of NiCl2 in MeOH; ppt. is filtered off, washed (MeOH containing a small amt. of ligand). dried in vac.; elem. anal.;

DOI:10.1016/S0020-1693(00)96018-3

Reference yield:

4-Benzoylpyridine (14548-46-0) + nickel dichloride (83864-14-6) → dichloro-tetra(4-benzoyl-pyridine)nickel(II) (99837-09-9)

Guidance literature:

In methanol; filtered off; washed with MeOH containing a small amount of 4-benzoyl-pyridine; dried in vac.; elem. anal.;

Reference yield:

dichloro-tetra(4-benzoyl-pyridine)nickel(II) (99837-09-9) → dichlorodi(4-benzoyl-pyridine)nickel(II)

Guidance literature:

In neat (no solvent); byproducts: 4-benzoylpyridine; controlled thermal decompn. of the Ni complex at 180°C;

DOI:10.1016/S0020-1693(00)96018-3

upstream raw materials:

4-Benzoylpyridine

nickel dichloride