(9,9-dimethyl-4,5-bis(diphenylphosphino)xanthene dioxide)diiodochlorocarbonylrhodium(III)

Base Information

• Chemical Name: (9,9-dimethyl-4,5-bis(diphenylphosphino)xanthene dioxide)diiodochlorocarbonylrhodium(III)
• CAS No.: 1241951-77-8
• Molecular Formula: C₄₀H₃₂ClI₂O₄P₂Rh
• Molecular Weight: 1030.81
• Mol file: 1241951-77-8.mol

Synonyms:

Chemical Property of (9,9-dimethyl-4,5-bis(diphenylphosphino)xanthene dioxide)diiodochlorocarbonylrhodium(III)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of (9,9-dimethyl-4,5-bis(diphenylphosphino)xanthene dioxide)diiodochlorocarbonylrhodium(III)

There total 1 articles about (9,9-dimethyl-4,5-bis(diphenylphosphino)xanthene dioxide)diiodochlorocarbonylrhodium(III) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(9,9-dimethyl-4,5-bis(diphenylphosphino)xanthene dioxide)chlorodicarbonylrhodium(I) (1241951-64-3) + iodine (7553-56-2,12190-71-5,8031-47-8) → (9,9-dimethyl-4,5-bis(diphenylphosphino)xanthene dioxide)diiodochlorocarbonylrhodium(III) (1241951-77-8)

Guidance literature:

In CH₂Cl₂; Rh complex dissolved in CH2Cl2, treated with soln. of I2, stirred at room temp. for 4 h; evapd.(vac.), washed (hexane);

DOI:10.1016/j.molcata.2010.05.008

upstream raw materials:

(9,9-dimethyl-4,5-bis(diphenylphosphino)xanthene dioxide)chlorodicarbonylrhodium(I)

iodine