6-[1-Phenyl-meth-(E)-ylidene]-cyclohex-1-enecarboxylic acid diisopropylamide

Base Information

• Chemical Name: 6-[1-Phenyl-meth-(E)-ylidene]-cyclohex-1-enecarboxylic acid diisopropylamide
• CAS No.: 80997-66-6
• Molecular Formula: C₂₀H₂₇NO
• Molecular Weight: 297.44
• Mol file: 80997-66-6.mol

Synonyms:

Chemical Property of 6-[1-Phenyl-meth-(E)-ylidene]-cyclohex-1-enecarboxylic acid diisopropylamide

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of 6-[1-Phenyl-meth-(E)-ylidene]-cyclohex-1-enecarboxylic acid diisopropylamide

There total 1 articles about 6-[1-Phenyl-meth-(E)-ylidene]-cyclohex-1-enecarboxylic acid diisopropylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N,N-diisopropyl-6-(trimethylsilyl)-1-cyclohexenecarboxamide (80997-59-7) + benzaldehyde (100-52-7) → 6-[1-Phenyl-meth-(E)-ylidene]-cyclohex-1-enecarboxylic acid diisopropylamide (80997-66-6) + 6-(Hydroxy-phenyl-methyl)-2-trimethylsilanyl-cyclohex-1-enecarboxylic acid diisopropylamide (80997-65-5)

Guidance literature:

With N,N,N,N,-tetramethylethylenediamine; sec.-butyllithium; Yield given. Multistep reaction. Yields of byproduct given; 1.) THF, -78 deg C, 5 min, 2.) from -78 deg C to RT;

DOI:10.1021/jo00347a060

upstream raw materials:

N,N-diisopropyl-6-(trimethylsilyl)-1-cyclohexenecarboxamide

benzaldehyde