4-<(2-hydroxymethyl-1-pyrrolidinyl)carbonyl>-3-methyl-5isoxazole

Base Information

• Chemical Name: 4-<(2-hydroxymethyl-1-pyrrolidinyl)carbonyl>-3-methyl-5isoxazole
• CAS No.: 132611-35-9
• Molecular Formula: C₂₃H₂₄N₂O₃S₂
• Molecular Weight: 440.587
• Mol file: 132611-35-9.mol

Synonyms:

Chemical Property of 4-<(2-hydroxymethyl-1-pyrrolidinyl)carbonyl>-3-methyl-5isoxazole

Chemical Property:

Purity/Quality:

Safty Information:

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Useful:

Technology Process of 4-<(2-hydroxymethyl-1-pyrrolidinyl)carbonyl>-3-methyl-5isoxazole

There total 1 articles about 4-<(2-hydroxymethyl-1-pyrrolidinyl)carbonyl>-3-methyl-5isoxazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-<(2-hydroxymethyl-1-pyrrolidinyl)carbonyl>-3,5-dimethylisoxazole (113317-82-1) + diphenyldisulfane (882-33-7) → 4-<(2-hydroxymethyl-1-pyrrolidinyl)carbonyl>-3-methyl-5isoxazole (132611-35-9)

Guidance literature:

With n-butyllithium; Yield given. Multistep reaction; 1) hexane/THF, -78 deg C 2 h 2) THF, -78 deg C 2 h;

DOI:10.1055/s-1990-27099

upstream raw materials:

4-<(2-hydroxymethyl-1-pyrrolidinyl)carbonyl>-3,5-dimethylisoxazole

diphenyldisulfane