2-{2-[(4-Methoxyphenyl)methoxy]ethyl}oxirane

Base Information

Chemical Name:2-{2-[(4-Methoxyphenyl)methoxy]ethyl}oxirane
CAS No.:142860-84-2
Molecular Formula:C12H16O3
Molecular Weight:208.257
Hs Code.:
DSSTox Substance ID:DTXSID00573820
Nikkaji Number:J2.568.122C

Synonyms:142860-84-2;2-{2-[(4-Methoxyphenyl)methoxy]ethyl}oxirane;SCHEMBL5854038;DTXSID00573820

Suppliers and Price of 2-{2-[(4-Methoxyphenyl)methoxy]ethyl}oxirane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-{2-[(4-Methoxyphenyl)methoxy]ethyl}oxirane

Chemical Property:

Boiling Point:301.1±17.0 °C(Predicted)
PSA：30.99000
Density:1.099±0.06 g/cm3(Predicted)
LogP:2.00070
XLogP3:1.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:6
Exact Mass:208.109944368
Heavy Atom Count:15
Complexity:176

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:COC1=CC=C(C=C1)COCCC2CO2

Technology Process of 2-{2-[(4-Methoxyphenyl)methoxy]ethyl}oxirane

There total 5 articles about 2-{2-[(4-Methoxyphenyl)methoxy]ethyl}oxirane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 142860-83-1
1-(4-methoxybenzyloxy)-3-butene

: 142860-84-2
4-(p-methoxybenzyloxy)-1,2-epoxybutane

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 20 ℃; for 8h;
DOI:10.1002/ejoc.200700868

Reference yield:

: 824-94-2
p-methoxybenzyl chloride

: 142860-84-2
4-(p-methoxybenzyloxy)-1,2-epoxybutane

Guidance literature:: Multi-step reaction with 2 steps

1.1: NaH / dimethylformamide / 10 h / 0 °C

1.2: dimethylformamide / 20 °C

2.1: 26.6 g / m-chloroperbenzoic acid / CH₂Cl₂

With sodium hydride; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja036521e

Reference yield:

: 2746-25-0
p-Methoxybenzyl bromide

: 142860-84-2
4-(p-methoxybenzyloxy)-1,2-epoxybutane

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / tetrahydrofuran / 0.5 h / 0 - 20 °C / Inert atmosphere

1.2: 17 h / 0 - 20 °C / Inert atmosphere

2.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 15 h / 0 - 20 °C / Inert atmosphere

With sodium hydride; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; dichloromethane;
DOI:10.1002/chem.201203965