zinc meso-triphenyltetrabenzoazaporphyrin

Base Information

• Chemical Name: zinc meso-triphenyltetrabenzoazaporphyrin
• CAS No.: 869644-58-6
• Molecular Formula: C₅₃H₃₁N₅Zn
• Molecular Weight: 803.253
• Mol file: 869644-58-6.mol

Synonyms:

Chemical Property of zinc meso-triphenyltetrabenzoazaporphyrin

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of zinc meso-triphenyltetrabenzoazaporphyrin

There total 1 articles about zinc meso-triphenyltetrabenzoazaporphyrin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 11.0%

phenylacetic acid (103-82-2) + isoindole-1,3-diylidenediamine (160956-25-2,160956-26-3,160956-27-4,160956-28-5,160956-29-6) + zinc(II) oxide → zinc meso-phenyltetrabenzotriazaporphyrin (869644-61-1) + zinc meso-cis-diphenyltetrabenzodiazaporphyrin (869644-59-7) + zinc meso-trans-diphenyltetrabenzodiazaporphyrin (869644-60-0) + zinc meso-triphenyltetrabenzoazaporphyrin (869644-58-6)

Guidance literature:

With potassium hydroxide; In melt; a mixt. of isoindoline-1,3-diimine, phenylacetic acid, and zinc oxide was heated in a quartz tube at 280°C for 1 h; the melt was cooled, ground and refluxed for 10 min in aq. KOH soln.; the melt was cooled, ground, refluxed for 10 min in aq. KOH soln., filtered off, washed with water to neutral washings, and dried; column chromy. (alumina, eluent: toluene-acetone, 10:1); elem. anal.;

DOI:10.1007/s11176-005-0289-8

upstream raw materials:

phenylacetic acid

isoindole-1,3-diylidenediamine