[diethyl 1a,9a,10a,18a-tetrahydro-3,8,12,17-tetrakis(2,3,4,5,6-pentafluorophenyl)-1H,10H,19H,21H-dicyclopropa[b,l]porphine-1,10-dicarboxylato(2-)-κN19,κN20,κN21,κN22]zinc

Base Information

Chemical Name:[diethyl 1a,9a,10a,18a-tetrahydro-3,8,12,17-tetrakis(2,3,4,5,6-pentafluorophenyl)-1H,10H,19H,21H-dicyclopropa[b,l]porphine-1,10-dicarboxylato(2-)-κN19,κN20,κN21,κN22]zinc
CAS No.:1125854-84-3
Molecular Formula:C₅₂H₂₀F₂₀N₄O₄Zn
Molecular Weight:1210.11
Hs Code.:

[diethyl 1a,9a,10a,18a-tetrahydro-3,8,12,17-tetrakis(2,3,4,5,6-pentafluorophenyl)-1H,10H,19H,21H-dicyclopropa[b,l]porphine-1,10-dicarboxylato(2-)-κN19,κN20,κN21,κN22]zinc

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Chemical Property of [diethyl 1a,9a,10a,18a-tetrahydro-3,8,12,17-tetrakis(2,3,4,5,6-pentafluorophenyl)-1H,10H,19H,21H-dicyclopropa[b,l]porphine-1,10-dicarboxylato(2-)-κN19,κN20,κN21,κN22]zinc

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Technology Process of [diethyl 1a,9a,10a,18a-tetrahydro-3,8,12,17-tetrakis(2,3,4,5,6-pentafluorophenyl)-1H,10H,19H,21H-dicyclopropa[b,l]porphine-1,10-dicarboxylato(2-)-κN19,κN20,κN21,κN22]zinc

There total 1 articles about [diethyl 1a,9a,10a,18a-tetrahydro-3,8,12,17-tetrakis(2,3,4,5,6-pentafluorophenyl)-1H,10H,19H,21H-dicyclopropa[b,l]porphine-1,10-dicarboxylato(2-)-κN19,κN20,κN21,κN22]zinc which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 623-73-4
diazoacetic acid ethyl ester

: 72076-08-5
5,10,15,20-tetrakis(pentafluorophenyl)porphyrin zinc(II)

: [ethyl (1α,1aβ,19aβ)-1a,19a-dihydro-3,8,13,18-tetrakis(2,3,4,5,6-pentafluorophenyl)-1H,20H,22H-cyclopropa[b]porphine-1-carboxylato(2-)-κN20,κN21,κN22,κN23]zinc

: [ethyl (1α,1aα,19aα)-1a,19a-dihydro-3,8,13,18-tetrakis(2,3,4,5,6-pentafluorophenyl)-1H,20H,22H-cyclopropa[b]porphine-1-carboxylato(2-)-κN20,κN21,κN22,κN23]zinc

: 1125854-84-3
[diethyl 1a,9a,10a,18a-tetrahydro-3,8,12,17-tetrakis(2,3,4,5,6-pentafluorophenyl)-1H,10H,19H,21H-dicyclopropa[b,l]porphine-1,10-dicarboxylato(2-)-κN19,κN20,κN21,κN22]zinc

: [diethyl 1a,4a,5a,18a-tetrahydro-3,7,12,17-tetrakis(2,3,4,5,6-pentafluorophenyl)-1H,5H,19H,21H-dicyclopropa[b,g]porphine-1,5-dicarboxylato(2-)-κN19,κN20,κN21,κN22]zinc

: [diethyl 1a,4a,5a,18a-tetrahydro-3,7,12,17-tetrakis(2,3,4,5,6-pentafluorophenyl)-1H,5H,19H,21H-dicyclopropa[b,g]porphine-1,5-dicarboxylato(2-)-κN19,κN20,κN21,κN22]zinc

Guidance literature:: copper(l) chloride; In dichloromethane; C2H5O2CCHN2 added dropwise during 7 h to a soln. of Zn complex and Cu compd. at 40°C under N2, stirred at 40°C for 12 h; evapd., flash-chromd. (silica gel, CH2Cl2/hexane), chromd. (TLC);
DOI:10.1002/hlca.200890247