IrCl₂(NH₂NH₂)PC₆H₅(OC₂H₅)2(As(C₆H₅)3)2⁽¹⁺⁾*B(C₆H₅)4^(1-)=[IrCl₂(NH₂NH₂)(PC₆H₅(OC₂H₅)2)(As(C₆H₅)3)2]B(C₆H₅)4

Base Information

• Chemical Name: IrCl₂(NH₂NH₂)PC₆H₅(OC₂H₅)2(As(C₆H₅)3)2⁽¹⁺⁾*B(C₆H₅)4^(1-)=[IrCl₂(NH₂NH₂)(PC₆H₅(OC₂H₅)2)(As(C₆H₅)3)2]B(C₆H₅)4
• CAS No.: 273922-48-8
• Molecular Formula: C₂₄H₂₀B*C₄₆H₄₉As₂Cl₂IrN₂O₂P
• Molecular Weight: 1425.08
• Mol file: 273922-48-8.mol

Synonyms:

Chemical Property of IrCl₂(NH₂NH₂)PC₆H₅(OC₂H₅)2(As(C₆H₅)3)2⁽¹⁺⁾*B(C₆H₅)4^(1-)=[IrCl₂(NH₂NH₂)(PC₆H₅(OC₂H₅)2)(As(C₆H₅)3)2]B(C₆H₅)4

Chemical Property:

Purity/Quality:

Safty Information:

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Useful:

Technology Process of IrCl₂(NH₂NH₂)PC₆H₅(OC₂H₅)2(As(C₆H₅)3)2⁽¹⁺⁾*B(C₆H₅)4^(1-)=[IrCl₂(NH₂NH₂)(PC₆H₅(OC₂H₅)2)(As(C₆H₅)3)2]B(C₆H₅)4

There total 1 articles about IrCl₂(NH₂NH₂)PC₆H₅(OC₂H₅)2(As(C₆H₅)3)2⁽¹⁺⁾*B(C₆H₅)4^(1-)=[IrCl₂(NH₂NH₂)(PC₆H₅(OC₂H₅)2)(As(C₆H₅)3)2]B(C₆H₅)4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

[IrHCl2(PC6H5(OC2H5)2)(As(C6H5)3)2] (273922-27-3) + sodium tetraphenyl borate (143-66-8) + hydrazine (302-01-2,78206-91-4,119775-10-9,75013-58-0) → IrCl2(NH2NH2)PC6H5(OC2H5)2(As(C6H5)3)2(1+)*B(C6H5)4(1-)=[IrCl2(NH2NH2)(PC6H5(OC2H5)2)(As(C6H5)3)2]B(C6H5)4 (273922-48-8)

Guidance literature:

With CF₃SO₃H; In dichloromethane; under inert atm.; addn. of equimolar amt. of CF3SO3H to soln. of Ir-complex in CH2Cl2 at -80°C, mixt. was brought to room temp., stirred for 1 h, excess of hydrazine was added, stirred for 2-3 h; solvent was removed under reduced pressure, triturated with EtOH containing an excess of NaBPh4, ppt. filtered off, crystd. from CH2Cl2/EtOH; elem. anal.;

DOI:10.1039/a909404k

upstream raw materials:

[IrHCl₂(PC₆H₅(OC₂H₅)2)(As(C₆H₅)3)2]

sodium tetraphenyl borate

hydrazine