Cr(CO)5Si(C₆H₄CH₂N(CH₃)2)2

Base Information

Chemical Name:Cr(CO)5Si(C₆H₄CH₂N(CH₃)2)2
CAS No.:135394-62-6
Molecular Formula:C₂₃H₂₄CrN₂O₅Si
Molecular Weight:488.535
Hs Code.:

Cr(CO)5Si(C<sub>6</sub>H<sub>4</sub>CH<sub>2</sub>N(CH<sub>3</sub>)2)2

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Chemical Property of Cr(CO)5Si(C₆H₄CH₂N(CH₃)2)2

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Technology Process of Cr(CO)5Si(C₆H₄CH₂N(CH₃)2)2

There total 2 articles about Cr(CO)5Si(C₆H₄CH₂N(CH₃)2)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

: disodium pentacarbonylchromium

: 135394-60-4
SiCl₂(C₆H₄CH₂N(CH₃)2)2

: 135394-62-6
Cr(CO)5Si(C₆H₄CH₂N(CH₃)2)2

Guidance literature:: In tetrahydrofuran; byproducts: NaCl; Na2Cr(CO)5 dissolved in THF (ultrasonic), soln. cooled to -40°C, silane soln. added with stirring; warmed to room temp. and stirred for 3h;; soln. separated from NaCl, concentrated in vac. (5E-2 Torr), crystd. at -20°C,;

Reference yield:

: disodium pentacarbonylchromium

: 135394-60-4
bis-(2-((dimethylamino)methyl)phenyl)dichlorosilane

: 135394-62-6
Cr(CO)5Si(C₆H₄CH₂N(CH₃)2)2

Guidance literature:: In tetrahydrofuran; under Ar; Na2Cr(CO)5 was dissolved in THF by ultrasonification, a soln. of the silane in THF was added at -40°C, warmed to room temp., stirred for 30 min; filtered, concd. in vac., crystd. at -20°C; elem anal.;