N-{N-[N-(N-benzyloxycarbonyl-D-alanyl)-glycyl]-D-alanyl}-glycine benzyl ester

Base Information

• Chemical Name: N-{N-[N-(N-benzyloxycarbonyl-D-alanyl)-glycyl]-D-alanyl}-glycine benzyl ester
• CAS No.: 103756-64-5
• Molecular Formula: C₂₅H₃₀N₄O₇
• Molecular Weight: 498.536
• Mol file: 103756-64-5.mol

Synonyms:

Chemical Property of N-{N-[N-(N-benzyloxycarbonyl-D-alanyl)-glycyl]-D-alanyl}-glycine benzyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-{N-[N-(N-benzyloxycarbonyl-D-alanyl)-glycyl]-D-alanyl}-glycine benzyl ester

There total 9 articles about N-{N-[N-(N-benzyloxycarbonyl-D-alanyl)-glycyl]-D-alanyl}-glycine benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-benzyloxycarbonylalanylglycine ethyl ester (4905-31-1) → N-{N-[N-(N-benzyloxycarbonyl-alanyl)-glycyl]-alanyl}-glycine benzyl ester (103756-64-5)

Guidance literature:

Multi-step reaction with 4 steps

1: ethanol; N₂H₄+H₂O

2: NaNO₂; aqueous HCl; acetic acid / Behandeln des Reaktionsprodukts mit DL-Alanin-aethylester

3: methanol; N₂H₄+H₂O

4: NaNO₂; aqueous HCl; acetic acid / Behandeln einer Suspension des Reaktionsprodukts in Aethylacetat mit Glycin-benzylester in CHCl₃

With hydrogenchloride; methanol; ethanol; hydrazine hydrate; acetic acid; sodium nitrite;

Reference yield:

N-[N-(N-benzyloxycarbonyl-alanyl)-glycyl]-alanine ethyl ester (110359-05-2) → N-{N-[N-(N-benzyloxycarbonyl-alanyl)-glycyl]-alanyl}-glycine benzyl ester (103756-64-5)

Guidance literature:

Multi-step reaction with 2 steps

1: methanol; N₂H₄+H₂O

2: NaNO₂; aqueous HCl; acetic acid / Behandeln einer Suspension des Reaktionsprodukts in Aethylacetat mit Glycin-benzylester in CHCl₃

With hydrogenchloride; methanol; hydrazine hydrate; acetic acid; sodium nitrite;

Reference yield:

N-(N-benzyloxycarbonyl-DL-alanyl)-glycine hydrazide (35660-90-3) → N-{N-[N-(N-benzyloxycarbonyl-alanyl)-glycyl]-alanyl}-glycine benzyl ester (103756-64-5)

Guidance literature:

Multi-step reaction with 3 steps

1: NaNO₂; aqueous HCl; acetic acid / Behandeln des Reaktionsprodukts mit DL-Alanin-aethylester

2: methanol; N₂H₄+H₂O

3: NaNO₂; aqueous HCl; acetic acid / Behandeln einer Suspension des Reaktionsprodukts in Aethylacetat mit Glycin-benzylester in CHCl₃

With hydrogenchloride; methanol; hydrazine hydrate; acetic acid; sodium nitrite;

upstream raw materials:

N-[N-(N-benzyloxycarbonyl-alanyl)-glycyl]-alanine hydrazide

N-benzyloxycarbonylalanylglycine ethyl ester

N-[N-(N-benzyloxycarbonyl-alanyl)-glycyl]-alanine ethyl ester

benzyloxycarbonylalanyl-glycine hydrazide