1L-N¹-benzyloxycarbonyl-O⁶-[2-benzyloxycarbonylamino-O⁴,O⁶-bis-(naphthalene-1-carbonyl)-α-D-ribo-2,3-dideoxy-hexopyranosyl]-N³,O⁴-carbonyl-2-deoxy-streptamine

Base Information

• Chemical Name: 1L-N¹-benzyloxycarbonyl-O⁶-[2-benzyloxycarbonylamino-O⁴,O⁶-bis-(naphthalene-1-carbonyl)-α-D-ribo-2,3-dideoxy-hexopyranosyl]-N³,O⁴-carbonyl-2-deoxy-streptamine
• CAS No.: 65456-89-5
• Molecular Formula: C₅₁H₄₇N₃O₁₃
• Molecular Weight: 909.946

Synonyms:

Chemical Property of 1L-N¹-benzyloxycarbonyl-O⁶-[2-benzyloxycarbonylamino-O⁴,O⁶-bis-(naphthalene-1-carbonyl)-α-D-ribo-2,3-dideoxy-hexopyranosyl]-N³,O⁴-carbonyl-2-deoxy-streptamine

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of 1L-N¹-benzyloxycarbonyl-O⁶-[2-benzyloxycarbonylamino-O⁴,O⁶-bis-(naphthalene-1-carbonyl)-α-D-ribo-2,3-dideoxy-hexopyranosyl]-N³,O⁴-carbonyl-2-deoxy-streptamine

There total 1 articles about 1L-N¹-benzyloxycarbonyl-O⁶-[2-benzyloxycarbonylamino-O⁴,O⁶-bis-(naphthalene-1-carbonyl)-α-D-ribo-2,3-dideoxy-hexopyranosyl]-N³,O⁴-carbonyl-2-deoxy-streptamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1D-N,N'-bis-benzyloxycarbonyl-O4-(2-benzyloxycarbonylamino-α-D-ribo-2,3-dideoxy-hexopyranosyl)-2-deoxy-streptamine (63532-10-5,73522-55-1) + naphthalene-1-carbonic acid chloride (879-18-5) → 1L-N1-benzyloxycarbonyl-O6-[2-benzyloxycarbonylamino-O4,O6-bis-(naphthalene-1-carbonyl)-α-D-ribo-2,3-dideoxy-hexopyranosyl]-N3,O4-carbonyl-2-deoxy-streptamine (65456-89-5)

Guidance literature:

Multistep reaction; (i) NaH, DMF, (ii) /BRN= 775785/, Py;

DOI:10.1246/bcsj.50.2369

Reference yield:

1L-N1-benzyloxycarbonyl-O6-[2-benzyloxycarbonylamino-O4,O6-bis-(naphthalene-1-carbonyl)-α-D-ribo-2,3-dideoxy-hexopyranosyl]-N3,O4-carbonyl-2-deoxy-streptamine (65456-89-5) + methanesulfonyl chloride (124-63-0) → 1L-N1-benzyloxycarbonyl-O6-[2-benzyloxycarbonylamino-O4,O6-bis-(naphthalene-1-carbonyl)-α-D-ribo-2,3-dideoxy-hexopyranosyl]-N3,O4-carbonyl-O5-methanesulfonyl-2-deoxy-streptamine (65456-90-8)

Guidance literature:

With pyridine; Ambient temperature;

DOI:10.1246/bcsj.50.2369

Reference yield:

1L-N1-benzyloxycarbonyl-O6-[2-benzyloxycarbonylamino-O4,O6-bis-(naphthalene-1-carbonyl)-α-D-ribo-2,3-dideoxy-hexopyranosyl]-N3,O4-carbonyl-2-deoxy-streptamine (65456-89-5) + methyl O5-benzoyl-O3-benzylsulfanylcarbonyl-O2-(4-nitro-benzoyl)-β-D-ribofuranoside (65456-97-5) → 1L-O5-[O5-benzoyl-O3-benzylsulfanylcarbonyl-O2-(4-nitro-benzoyl)-β-D-ribofuranosyl]-N1-benzyloxycarbonyl-O6-[2-benzyloxycarbonylamino-O4,O6-bis-(naphthalene-1-carbonyl)-α-D-ribo-2,3-dideoxy-hexopyranosyl]-N3,O4-carbonyl-2-deoxy-streptamine (65457-01-4)

Guidance literature:

Multistep reaction; (i) HBr, AcOH, CH₂Cl₂, (ii) /BRN= 1206859/, Hg(CN)2, CaSO₄;

DOI:10.1246/bcsj.50.2369

upstream raw materials:

1D-N,N'-bis-benzyloxycarbonyl-O⁴-(2-benzyloxycarbonylamino-α-D-ribo-2,3-dideoxy-hexopyranosyl)-2-deoxy-streptamine

naphthalene-1-carbonic acid chloride

Downstream raw materials:

1L-O⁵-[O⁵-benzoyl-O³-benzylsulfanylcarbonyl-O²-(4-nitro-benzoyl)-β-D-ribofuranosyl]-N¹-benzyloxycarbonyl-O⁶-[2-benzyloxycarbonylamino-O⁴,O⁶-bis-(naphthalene-1-carbonyl)-α-D-ribo-2,3-dideoxy-hexopyranosyl]-N³,O⁴-carbonyl-2-deoxy-streptamine

1L-N¹-benzyloxycarbonyl-O⁶-[2-benzyloxycarbonylamino-O⁴,O⁶-bis-(naphthalene-1-carbonyl)-α-D-ribo-2,3-dideoxy-hexopyranosyl]-N³,O⁴-carbonyl-O⁵-methanesulfonyl-2-deoxy-streptamine

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