1-(P-TOSYL)-3,4,4-TRIMETHYLIMIDAZOLIDINE

Base Information

Chemical Name:1-(P-TOSYL)-3,4,4-TRIMETHYLIMIDAZOLIDINE
CAS No.:73955-61-0
Molecular Formula:C13H20 N2 O2 S
Molecular Weight:268.38
Hs Code.:2933990090
European Community (EC) Number:633-317-3
DSSTox Substance ID:DTXSID30224691
Nikkaji Number:J307.925B
Wikidata:Q83103353
Mol file:73955-61-0.mol

Synonyms:1-(P-TOSYL)-3,4,4-TRIMETHYLIMIDAZOLIDINE

Suppliers and Price of 1-(P-TOSYL)-3,4,4-TRIMETHYLIMIDAZOLIDINE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
1-(P-TOSYL)-3,4,4-TRIMETHYLIMIDAZOLIDINE 95.00%
5G
$ 1015.08

Total 2 raw suppliers

Chemical Property of 1-(P-TOSYL)-3,4,4-TRIMETHYLIMIDAZOLIDINE

Chemical Property:

Vapor Pressure:1.33E-05mmHg at 25°C
Melting Point:66-67 °C(lit.)
Boiling Point:367.8°C at 760 mmHg
Flash Point:176.2°C
PSA：49.00000
Density:1.152g/cm³
LogP:2.62380
Storage Temp.:−20°C
XLogP3:2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:2
Exact Mass:268.12454906
Heavy Atom Count:18
Complexity:392

Purity/Quality:

98%Min ^*data from raw suppliers

1-(P-TOSYL)-3,4,4-TRIMETHYLIMIDAZOLIDINE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:Xi
Statements: 36/37/38
Safety Statements: 26-36

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

Canonical SMILES:CC1=CC=C(C=C1)S(=O)(=O)N2CC(N(C2)C)(C)C

Technology Process of 1-(P-TOSYL)-3,4,4-TRIMETHYLIMIDAZOLIDINE

There total 5 articles about 1-(P-TOSYL)-3,4,4-TRIMETHYLIMIDAZOLIDINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 71254-91-6
1-tosyl-3,4,4-trimethyl-Δ²-imidazolinium iodide

: 73955-61-0
1-tosyl-3,4,4-trimethyl-2-imidazolidine

Guidance literature:: With sodium tetrahydroborate; In ethanol; at 0 ℃; for 1h;
DOI:10.1016/S0040-4020(01)90903-2

Reference yield:

: 71254-89-2
1-p-toluenesulfonyl-4,4-dimethyl-Δ²-imidazoline

: 73955-61-0
1-tosyl-3,4,4-trimethyl-2-imidazolidine

Guidance literature:: Multi-step reaction with 2 steps

1: 76 percent / CH₂Cl₂ / Heating

2: 92 percent / NaBH₄ / ethanol / 1 h / 0 °C

With sodium tetrahydroborate; In ethanol; dichloromethane;
DOI:10.1016/S0040-4020(01)90903-2

Reference yield:

: 2305-59-1
4,4-dimethyl-2-imidazoline

: 73955-61-0
1-tosyl-3,4,4-trimethyl-2-imidazolidine

Guidance literature:: Multi-step reaction with 3 steps

1: 94 percent / triethylamine / CH₂Cl₂ / 0 deg C, then warming to RT, 1 h

2: 76 percent / CH₂Cl₂ / Heating

3: 92 percent / NaBH₄ / ethanol / 1 h / 0 °C

With sodium tetrahydroborate; triethylamine; In ethanol; dichloromethane;
DOI:10.1016/S0040-4020(01)90903-2