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Trimethylsiloxy-trimethylsilylmethyl-phenylsulphide

Base Information
  • Chemical Name:Trimethylsiloxy-trimethylsilylmethyl-phenylsulphide
  • CAS No.:129584-67-4
  • Molecular Formula:C13H24OSSi2
  • Molecular Weight:284.57
  • Hs Code.:
Trimethylsiloxy-trimethylsilylmethyl-phenylsulphide

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Chemical Property of Trimethylsiloxy-trimethylsilylmethyl-phenylsulphide
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Technology Process of Trimethylsiloxy-trimethylsilylmethyl-phenylsulphide

There total 1 articles about Trimethylsiloxy-trimethylsilylmethyl-phenylsulphide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With n-butyllithium; Yield given. Multistep reaction; 1.1) Et2O, hexane, -78 deg C, 1.2.) reflux, 3 h, 2.) -78 deg C to room temp.;
DOI:10.1016/S0040-4020(01)88391-5
Guidance literature:
With sodium hexamethyldisilazane; tetrabutyl ammonium fluoride; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts; 1.) THF, 0 deg C, 2.1) 15 min, -30 deg C, 2.2) 3 h, room temperature;
DOI:10.1016/S0040-4020(01)88391-5
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