2-cyclopropylidene-2-(2-bromo phenyl)-1-phenoxy ethane

Base Information

Chemical Name:2-cyclopropylidene-2-(2-bromo phenyl)-1-phenoxy ethane
CAS No.:188549-22-6
Molecular Formula:C₁₇H₁₅BrO
Molecular Weight:315.209
Hs Code.:

Synonyms:

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Chemical Property of 2-cyclopropylidene-2-(2-bromo phenyl)-1-phenoxy ethane

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Technology Process of 2-cyclopropylidene-2-(2-bromo phenyl)-1-phenoxy ethane

There total 3 articles about 2-cyclopropylidene-2-(2-bromo phenyl)-1-phenoxy ethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 49851-55-0
2,2'-dibromoacetophenone

: 188549-22-6
2-cyclopropylidene-2-(2-bromo phenyl)-1-phenoxy ethane

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / K₂CO₃ / 20 h / Heating

2: 1.) NaH, ethanol, 2.) tris<2-(2-methoxyethoxy)-ethyl>amine / 1.) THF, mineral oil, 65 deg C, 6 h, 2.) THF, mineral oil, 65 deg C, 14 h

With ethanol; Tris(3,6-dioxaheptyl)amine; sodium hydride; potassium carbonate;
DOI:10.1080/00397919708004192

Reference yield:

: 108-95-2,27073-41-2
phenol

: 188549-22-6
2-cyclopropylidene-2-(2-bromo phenyl)-1-phenoxy ethane

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / K₂CO₃ / 20 h / Heating

2: 1.) NaH, ethanol, 2.) tris<2-(2-methoxyethoxy)-ethyl>amine / 1.) THF, mineral oil, 65 deg C, 6 h, 2.) THF, mineral oil, 65 deg C, 14 h

With ethanol; Tris(3,6-dioxaheptyl)amine; sodium hydride; potassium carbonate;
DOI:10.1080/00397919708004192

Reference yield:

: 188549-17-9
1-(2-bromo phenyl)-2-phenoxy etanone

: 3607-17-8
3-bromopropyltriphenylphosphonium bromide

: 188549-22-6
2-cyclopropylidene-2-(2-bromo phenyl)-1-phenoxy ethane

Guidance literature:: With ethanol; Tris(3,6-dioxaheptyl)amine; sodium hydride; Yield given. Multistep reaction; 1.) THF, mineral oil, 65 deg C, 6 h, 2.) THF, mineral oil, 65 deg C, 14 h;
DOI:10.1080/00397919708004192